Temperature modulation in PDSC for monitoring the curing under pressure View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2011-10

AUTHORS

C. Gracia-Fernández, J. Tarrío-Saavedra, J. López-Beceiro, S. Gómez-Barreiro, S. Naya, R. Artiaga

ABSTRACT

The use of pressure cell attached to a temperature modulated differential scanning calorimeter (TMDSC) is investigated to perform modulated DSC experiments at high pressures (TMPDSC). No previous reports were found on the use of TMPDSC. In this study, the proposed method is applied to the study of the pressure effect on the curing reaction of an epoxy system. Curing quasi-isothermal modulated experiments were performed at different pressures to evaluate the vitrification time. Linear heating modulated tests were also successfully performed at different pressures to separate the reversing glass transition effect from the residual exothermic cure reaction. The curing enthalpy, conversion versus temperature, and glass transition of the fully cured thermoset were also evaluated. All the studied parameters resulted to be affected by the pressure in the range from atmospheric pressure to 35 bar. It was observed that the curing enthalpy, the reaction rate and the conversion at any given time increase with any pressure increment. The usefulness of TMDSC to characterize the curing of thermosets is extended by PTMDSC to situations, i.e., aeronautics industry, where pressure curing is needed. More... »

PAGES

101-107

References to SciGraph publications

  • 2001-09. Matching Cure Characteristics of Automotive Rubber Compound and Polyurethane Coating in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
  • 2006. Theory and Practice of Modulated Temperature Differential Scanning Calorimetry in MODULATED TEMPERATURE DIFFERENTIAL SCANNING CALORIMETRY
  • 2006. The Application of Modulated Temperature Differential Scanning Calorimetry for the Characterisation of Curing Systems in MODULATED TEMPERATURE DIFFERENTIAL SCANNING CALORIMETRY
  • 2010-12. A vitrification and curing study by simultaneous TMDSC-photocalorimetry in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
  • Identifiers

    URI

    http://scigraph.springernature.com/pub.10.1007/s10973-011-1361-8

    DOI

    http://dx.doi.org/10.1007/s10973-011-1361-8

    DIMENSIONS

    https://app.dimensions.ai/details/publication/pub.1015416585


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