Avrami exponent of crystallization in tellurite glasses View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2011-11

AUTHORS

S. M. Sidel, F. A. Santos, V. O. Gordo, E. Idalgo, A. A. Monteiro, J. C. S. Moraes, K. Yukimitu

ABSTRACT

Nucleation process and crystal growth for three samples of the (20-x)Li2O–80TeO2–xWO3 glass system were studied using X-ray diffraction and differential scanning calorimetry techniques. X-ray diffraction data confirmed the amorphous characteristic of the as-quenched samples and indicated the growth of crystalline phases formed due to the thermal treatment for annealed samples. These results reveal the presence of three distinct γ-TeO2, α-TeO2 and α-Li2Te2O5 crystalline phases in the TL sample, and two distinct α-TeO2 and γ-TeO2 crystalline phases in the TLW5 and TLW10 samples. The activation energy and the Avrami exponent were determined from DSC measurements. The activation energy values X-ray diffraction data of the TLW10 glass sample suggest that γ-TeO2 phase occur before the α-TeO2. The results obtained for the Avrami exponent point to that the nucleation process is volumetric and that the crystal growth is two or three-dimensional. More... »

PAGES

613-618

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10973-011-1312-4

DOI

http://dx.doi.org/10.1007/s10973-011-1312-4

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1047174797


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