Parameter estimation of kinetic cure using DSC non-isothermal data View Full Text


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Article Info

DATE

2011-02

AUTHORS

Rogério L. Pagano, Verônica M. A. Calado, Frederico W. Tavares, Evaristo C. Biscaia

ABSTRACT

In the present contribution, a procedure to estimate parameters using non-isothermal data was applied. The estimation procedure is based on the use of an energy balance in DSC furnace. The approach found all kinetic parameters of autocatalytic model (E1, E2, A1, A2, m, n) besides the ultimate reaction heat and their confidence regions by using deterministic and heuristic algorithms. The application of this approach to isothermal data was done in a previous work and similar results were obtained. The results show that the use of an energy balance is a good methodology to estimate cure kinetic parameters of non-isothermal experiments. More... »

PAGES

495-499

References to SciGraph publications

  • 2009-11. DSC studies on the curing kinetics of chitosan–alanine using glutaraldehyde as crosslinker in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
  • 2003-05. Simulation of isothermal cure of A powder coating in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
  • 2009-08. TG, EGA and kinetic study by non-isothermal decomposition of a polyaniline with different dispersion degree in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
  • 2009-09. Curing kinetics of lignin-novolac phenolic resins using non-isothermal methods in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
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    URI

    http://scigraph.springernature.com/pub.10.1007/s10973-010-0984-5

    DOI

    http://dx.doi.org/10.1007/s10973-010-0984-5

    DIMENSIONS

    https://app.dimensions.ai/details/publication/pub.1031442937


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