Kinetic parameters of unsaturated polyester resin modified with poly(ε -caprolactone) View Full Text


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Article Info

DATE

2006-12

AUTHORS

J. Escribano, R. Masegosa, D. Nava, M. G. Prolongo, Catalina Salom

ABSTRACT

The curing of the neat unsaturated polyester resin (UP) with benzoyl peroxide (initiator) as well as the curing of UP modified with two poly(ε-caprolactone) PCL samples (PCL2 and PCL50) of different molecular masses (Mn=2⋅103 and Mn=5⋅104, respectively), were investigated by non-isothermal differential scanning calorimetry (DSC), at different heating rates. The activation energy was determined from the variation of the peak exotherm temperature, Tpeak, upon heating rate. Besides, the degree of conversion (α) was obtained from isothermal DSC measurements at 80°C at different curing times for neat UP, UP+ PCL2 and UP+PCL50. Kinetic parameters were deduced assuming the nth order reaction kinetic model for neat UP, UP+PCL2 and UP+PCL50 systems. More... »

PAGES

675-679

References to SciGraph publications

  • 1985-11. Kinetic study of the cure reaction of unsaturated polyester resins in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
  • 1988-03. Influence of functional rubbers on the curing process of unsaturated polyester resins in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
  • 1970-09. Kinetic analysis of derivative curves in thermal analysis in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
  • 1999-09. Thermoset Cure Kinetics by Isoconversional Methods in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
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    http://scigraph.springernature.com/pub.10.1007/s10973-006-7892-8

    DOI

    http://dx.doi.org/10.1007/s10973-006-7892-8

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