Thermal decomposition of ammonium jarosite (NH4)Fe3(SO4)2(OH)6 View Full Text


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Article Info

DATE

2006-05

AUTHORS

Ray L. Frost, Rachael-Anne Wills, J. Theo Kloprogge, Wayde Martens

ABSTRACT

Thermogravimetry combined with mass spectrometry has been used to study the thermal decomposition of a synthetic ammonium jarosite. Five mass loss steps are observed at 120, 260, 389, 510 and 541°C. Mass spectrometry through evolved gases confirms these steps as loss of water, dehydroxylation, loss of ammonia and loss of sulphate in two steps. Changes in the molecular structure of the ammonium jarosite were followed by infrared emission spectroscopy (IES). This technique allows the infrared spectrum at the elevated temperatures to be obtained. IES confirms the dehydroxylation to have taken place by 300°C and the ammonia loss by 450°C. Loss of the sulphate is observed by changes in band position and intensity after 500°C. More... »

PAGES

489-496

References to SciGraph publications

  • 1998-12. A kinetic study of the thermal decomposition of ammoniojarosite in JOURNAL OF MATERIALS SCIENCE
  • 1980-10. Thermal analysis of iron(II) sulphate heptahydrate in air in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
  • 2003-02. DSC and high-resolution TG of synthesized hydrotalcites of Mg and Zn in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
  • 1979-04. Thermal analysis of ferrous sulphate heptahydrate in air in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
  • 2004-04. Thermal decomposition of synthetic hydrotalcites reevesite and pyroaurite in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
  • 2004-09. Thermal treatment of moolooite in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
  • 2004-10. Thermodynamic properties, low-temperature heat-capacity anomalies, and single-crystal X-ray refinement of hydronium jarosite, (H3O)Fe3(SO4)2(OH)6 in PHYSICS AND CHEMISTRY OF MINERALS
  • 1979-08. Thermal analysis of ferrous sulphate heptahydrate in air in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
  • 1996-10. The Dehydroxylation of the Kaolinite Clay Minerals using Infrared Emission Spectroscopy in CLAYS AND CLAY MINERALS
  • 1981-02. Thermal analysis of iron(II) sulphate heptahydrate in air. V in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
  • 2003-03. Thermal analysis of goethite in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
  • 2004-06. Thermal decomposition of struvite in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
  • 2004-01. Thermal decomposition of humboldtine: A high resolution thermogravimetric and hot stage Raman spectroscopic study in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
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    http://scigraph.springernature.com/pub.10.1007/s10973-005-6953-8

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    http://dx.doi.org/10.1007/s10973-005-6953-8

    DIMENSIONS

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