Raman study of the variation in anatase structure of TiO2 nanopowders due to the changes of sol–gel synthesis conditions View Full Text


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Article Info

DATE

2009-03

AUTHORS

A. Golubović, M. Šćepanović, A. Kremenović, S. Aškrabić, V. Berec, Z. Dohčević-Mitrović, Z. V. Popović

ABSTRACT

TiO2 nanopowders were produced by sol–gel technique under different synthesis conditions. XRD results have shown that obtained nanopowders are in anatase phase, with the presence of a small amount of highly disordered brookite phase, whereas nanocrystallite size and amount of brookite slightly depend on sol–gel synthesis conditions. Raman measurements confirm these results. The analyses of the shift and width of the most intensive anatase Eg Raman mode by phonon confinement model suggest that anatase crystallite size should be in the range between 11 and 15 nm, what is in excellent correlation with XRD results. Obtained results have shown that Raman spectroscopy is a highly sensitive method for the estimation of anatase crystallite size as well as brookite content in TiO2 nanopowders synthesized by variable sol–gel synthesis conditions. More... »

PAGES

311

References to SciGraph publications

  • 2006-10. Microwave processing of TiO2 blocking layers for dye-sensitized solar cells in JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY
  • 2007-03. Temperature dependence of the lowest frequency Eg Raman mode in laser-synthesized anatase TiO2 nanopowder in APPLIED PHYSICS A
  • 2006-02. Current sol-gel activities in Japan in JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY
  • 1998-01. A Raman Scattering Study of PbTiO3 and TiO2 Obtained by Sol-Gel in JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY
  • Identifiers

    URI

    http://scigraph.springernature.com/pub.10.1007/s10971-008-1872-3

    DOI

    http://dx.doi.org/10.1007/s10971-008-1872-3

    DIMENSIONS

    https://app.dimensions.ai/details/publication/pub.1006023061


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