Low-temperature preparation of nanocrystalline anatase films through a sol-gel route View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2006-09

AUTHORS

Margit J. Jensen, Paul A. Fuierer

ABSTRACT

Nanocrystalline anatase (TiO2) films were prepared at very low temperature through a sol-gel route using titanium isopropoxide and hydrogen peroxide in ethanol. Crystallization occurred after film deposition at 35°C in an atmosphere saturated with water vapor. Both thin and thick films of nanocrystalline anatase were prepared. Observed particle size in crystallized films is approximately 20–40 nm as measured with AFM. No residual organic material was apparent through FTIR after crystallization occurred. Dynamic light scattering studies performed on this system indicate that particle size measured in solution is strongly dependent on the amount of agitation samples received prior to measurement. More... »

PAGES

229-233

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10971-006-7837-5

DOI

http://dx.doi.org/10.1007/s10971-006-7837-5

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1039768814


Indexing Status Check whether this publication has been indexed by Scopus and Web Of Science using the SN Indexing Status Tool
Incoming Citations Browse incoming citations for this publication using opencitations.net

JSON-LD is the canonical representation for SciGraph data.

TIP: You can open this SciGraph record using an external JSON-LD service: JSON-LD Playground Google SDTT

[
  {
    "@context": "https://springernature.github.io/scigraph/jsonld/sgcontext.json", 
    "about": [
      {
        "id": "http://purl.org/au-research/vocabulary/anzsrc-for/2008/0306", 
        "inDefinedTermSet": "http://purl.org/au-research/vocabulary/anzsrc-for/2008/", 
        "name": "Physical Chemistry (incl. Structural)", 
        "type": "DefinedTerm"
      }, 
      {
        "id": "http://purl.org/au-research/vocabulary/anzsrc-for/2008/03", 
        "inDefinedTermSet": "http://purl.org/au-research/vocabulary/anzsrc-for/2008/", 
        "name": "Chemical Sciences", 
        "type": "DefinedTerm"
      }
    ], 
    "author": [
      {
        "affiliation": {
          "alternateName": "New Mexico Institute of Mining and Technology", 
          "id": "https://www.grid.ac/institutes/grid.39679.32", 
          "name": [
            "Department of Materials Science and Engineering, New Mexico Institute of Mining and Technology, 801 Leroy Place, 87801, Socorro, NM"
          ], 
          "type": "Organization"
        }, 
        "familyName": "Jensen", 
        "givenName": "Margit J.", 
        "type": "Person"
      }, 
      {
        "affiliation": {
          "alternateName": "New Mexico Institute of Mining and Technology", 
          "id": "https://www.grid.ac/institutes/grid.39679.32", 
          "name": [
            "Department of Materials Science and Engineering, New Mexico Institute of Mining and Technology, 801 Leroy Place, 87801, Socorro, NM"
          ], 
          "type": "Organization"
        }, 
        "familyName": "Fuierer", 
        "givenName": "Paul A.", 
        "id": "sg:person.0643673614.17", 
        "sameAs": [
          "https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.0643673614.17"
        ], 
        "type": "Person"
      }
    ], 
    "citation": [
      {
        "id": "https://doi.org/10.1016/0378-7753(85)88026-5", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1013387500"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "sg:pub.10.1023/a:1018332221696", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1013824585", 
          "https://doi.org/10.1023/a:1018332221696"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "sg:pub.10.1038/353737a0", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1014356537", 
          "https://doi.org/10.1038/353737a0"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "https://doi.org/10.1111/j.1151-2916.2000.tb01178.x", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1018903570"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "https://doi.org/10.1016/0040-6090(94)06401-6", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1025109850"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "sg:pub.10.1038/35104607", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1025421157", 
          "https://doi.org/10.1038/35104607"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "sg:pub.10.1038/35104607", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1025421157", 
          "https://doi.org/10.1038/35104607"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "sg:pub.10.1007/s10971-005-2521-8", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1028006782", 
          "https://doi.org/10.1007/s10971-005-2521-8"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "sg:pub.10.1007/s10971-005-2521-8", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1028006782", 
          "https://doi.org/10.1007/s10971-005-2521-8"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "https://doi.org/10.1006/jcis.2002.8371", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1029059447"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "https://doi.org/10.1006/jcat.2001.3316", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1032146733"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "https://doi.org/10.1016/0013-4686(82)80146-1", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1034171332"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "sg:pub.10.1023/a:1023754718688", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1042932221", 
          "https://doi.org/10.1023/a:1023754718688"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "https://doi.org/10.1149/1.2048726", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1043058640"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "sg:pub.10.1023/a:1015305328932", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1044107632", 
          "https://doi.org/10.1023/a:1015305328932"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "https://doi.org/10.1021/ie0498551", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1055598639"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "https://doi.org/10.1021/ie0498551", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1055598639"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "https://doi.org/10.1021/ja954172l", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1055864300"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "https://doi.org/10.1021/ja954172l", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1055864300"
        ], 
        "type": "CreativeWork"
      }
    ], 
    "datePublished": "2006-09", 
    "datePublishedReg": "2006-09-01", 
    "description": "Nanocrystalline anatase (TiO2) films were prepared at very low temperature through a sol-gel route using titanium isopropoxide and hydrogen peroxide in ethanol. Crystallization occurred after film deposition at 35\u00b0C in an atmosphere saturated with water vapor. Both thin and thick films of nanocrystalline anatase were prepared. Observed particle size in crystallized films is approximately 20\u201340 nm as measured with AFM. No residual organic material was apparent through FTIR after crystallization occurred. Dynamic light scattering studies performed on this system indicate that particle size measured in solution is strongly dependent on the amount of agitation samples received prior to measurement.", 
    "genre": "research_article", 
    "id": "sg:pub.10.1007/s10971-006-7837-5", 
    "inLanguage": [
      "en"
    ], 
    "isAccessibleForFree": false, 
    "isPartOf": [
      {
        "id": "sg:journal.1048337", 
        "issn": [
          "0928-0707", 
          "1573-4846"
        ], 
        "name": "Journal of Sol-Gel Science and Technology", 
        "type": "Periodical"
      }, 
      {
        "issueNumber": "3", 
        "type": "PublicationIssue"
      }, 
      {
        "type": "PublicationVolume", 
        "volumeNumber": "39"
      }
    ], 
    "name": "Low-temperature preparation of nanocrystalline anatase films through a sol-gel route", 
    "pagination": "229-233", 
    "productId": [
      {
        "name": "readcube_id", 
        "type": "PropertyValue", 
        "value": [
          "bd710704a73c734708b6b9232c91b8c3237e64bacc97ceea87fa3c4deaaf4f2a"
        ]
      }, 
      {
        "name": "doi", 
        "type": "PropertyValue", 
        "value": [
          "10.1007/s10971-006-7837-5"
        ]
      }, 
      {
        "name": "dimensions_id", 
        "type": "PropertyValue", 
        "value": [
          "pub.1039768814"
        ]
      }
    ], 
    "sameAs": [
      "https://doi.org/10.1007/s10971-006-7837-5", 
      "https://app.dimensions.ai/details/publication/pub.1039768814"
    ], 
    "sdDataset": "articles", 
    "sdDatePublished": "2019-04-11T00:16", 
    "sdLicense": "https://scigraph.springernature.com/explorer/license/", 
    "sdPublisher": {
      "name": "Springer Nature - SN SciGraph project", 
      "type": "Organization"
    }, 
    "sdSource": "s3://com-uberresearch-data-dimensions-target-20181106-alternative/cleanup/v134/2549eaecd7973599484d7c17b260dba0a4ecb94b/merge/v9/a6c9fde33151104705d4d7ff012ea9563521a3ce/jats-lookup/v90/0000000001_0000000264/records_8695_00000514.jsonl", 
    "type": "ScholarlyArticle", 
    "url": "http://link.springer.com/10.1007%2Fs10971-006-7837-5"
  }
]
 

Download the RDF metadata as:  json-ld nt turtle xml License info

HOW TO GET THIS DATA PROGRAMMATICALLY:

JSON-LD is a popular format for linked data which is fully compatible with JSON.

curl -H 'Accept: application/ld+json' 'https://scigraph.springernature.com/pub.10.1007/s10971-006-7837-5'

N-Triples is a line-based linked data format ideal for batch operations.

curl -H 'Accept: application/n-triples' 'https://scigraph.springernature.com/pub.10.1007/s10971-006-7837-5'

Turtle is a human-readable linked data format.

curl -H 'Accept: text/turtle' 'https://scigraph.springernature.com/pub.10.1007/s10971-006-7837-5'

RDF/XML is a standard XML format for linked data.

curl -H 'Accept: application/rdf+xml' 'https://scigraph.springernature.com/pub.10.1007/s10971-006-7837-5'


 

This table displays all metadata directly associated to this object as RDF triples.

118 TRIPLES      21 PREDICATES      42 URIs      19 LITERALS      7 BLANK NODES

Subject Predicate Object
1 sg:pub.10.1007/s10971-006-7837-5 schema:about anzsrc-for:03
2 anzsrc-for:0306
3 schema:author Nc3f3968c475c48588f6e44a0d3a06d1a
4 schema:citation sg:pub.10.1007/s10971-005-2521-8
5 sg:pub.10.1023/a:1015305328932
6 sg:pub.10.1023/a:1018332221696
7 sg:pub.10.1023/a:1023754718688
8 sg:pub.10.1038/35104607
9 sg:pub.10.1038/353737a0
10 https://doi.org/10.1006/jcat.2001.3316
11 https://doi.org/10.1006/jcis.2002.8371
12 https://doi.org/10.1016/0013-4686(82)80146-1
13 https://doi.org/10.1016/0040-6090(94)06401-6
14 https://doi.org/10.1016/0378-7753(85)88026-5
15 https://doi.org/10.1021/ie0498551
16 https://doi.org/10.1021/ja954172l
17 https://doi.org/10.1111/j.1151-2916.2000.tb01178.x
18 https://doi.org/10.1149/1.2048726
19 schema:datePublished 2006-09
20 schema:datePublishedReg 2006-09-01
21 schema:description Nanocrystalline anatase (TiO2) films were prepared at very low temperature through a sol-gel route using titanium isopropoxide and hydrogen peroxide in ethanol. Crystallization occurred after film deposition at 35°C in an atmosphere saturated with water vapor. Both thin and thick films of nanocrystalline anatase were prepared. Observed particle size in crystallized films is approximately 20–40 nm as measured with AFM. No residual organic material was apparent through FTIR after crystallization occurred. Dynamic light scattering studies performed on this system indicate that particle size measured in solution is strongly dependent on the amount of agitation samples received prior to measurement.
22 schema:genre research_article
23 schema:inLanguage en
24 schema:isAccessibleForFree false
25 schema:isPartOf N4f9b7bb449164a00bc81a1e73ac99f6e
26 Nd47e043ff0c24e449c338872220de200
27 sg:journal.1048337
28 schema:name Low-temperature preparation of nanocrystalline anatase films through a sol-gel route
29 schema:pagination 229-233
30 schema:productId N3aa4c244842a4d07bf136c08861cf19e
31 N3fa77beb87eb4d41a0efe02f61992594
32 Na5d373c51d48407292e753dd9ef6cd48
33 schema:sameAs https://app.dimensions.ai/details/publication/pub.1039768814
34 https://doi.org/10.1007/s10971-006-7837-5
35 schema:sdDatePublished 2019-04-11T00:16
36 schema:sdLicense https://scigraph.springernature.com/explorer/license/
37 schema:sdPublisher N12692a44f17d4edea0ee1367506f82a1
38 schema:url http://link.springer.com/10.1007%2Fs10971-006-7837-5
39 sgo:license sg:explorer/license/
40 sgo:sdDataset articles
41 rdf:type schema:ScholarlyArticle
42 N12692a44f17d4edea0ee1367506f82a1 schema:name Springer Nature - SN SciGraph project
43 rdf:type schema:Organization
44 N3aa4c244842a4d07bf136c08861cf19e schema:name readcube_id
45 schema:value bd710704a73c734708b6b9232c91b8c3237e64bacc97ceea87fa3c4deaaf4f2a
46 rdf:type schema:PropertyValue
47 N3fa77beb87eb4d41a0efe02f61992594 schema:name doi
48 schema:value 10.1007/s10971-006-7837-5
49 rdf:type schema:PropertyValue
50 N4f9b7bb449164a00bc81a1e73ac99f6e schema:volumeNumber 39
51 rdf:type schema:PublicationVolume
52 N8d6274165e174bed963cdd0a3b198454 rdf:first sg:person.0643673614.17
53 rdf:rest rdf:nil
54 Na5d373c51d48407292e753dd9ef6cd48 schema:name dimensions_id
55 schema:value pub.1039768814
56 rdf:type schema:PropertyValue
57 Nc3f3968c475c48588f6e44a0d3a06d1a rdf:first Nf22ca60b81a04a6f9b6a829738d4f934
58 rdf:rest N8d6274165e174bed963cdd0a3b198454
59 Nd47e043ff0c24e449c338872220de200 schema:issueNumber 3
60 rdf:type schema:PublicationIssue
61 Nf22ca60b81a04a6f9b6a829738d4f934 schema:affiliation https://www.grid.ac/institutes/grid.39679.32
62 schema:familyName Jensen
63 schema:givenName Margit J.
64 rdf:type schema:Person
65 anzsrc-for:03 schema:inDefinedTermSet anzsrc-for:
66 schema:name Chemical Sciences
67 rdf:type schema:DefinedTerm
68 anzsrc-for:0306 schema:inDefinedTermSet anzsrc-for:
69 schema:name Physical Chemistry (incl. Structural)
70 rdf:type schema:DefinedTerm
71 sg:journal.1048337 schema:issn 0928-0707
72 1573-4846
73 schema:name Journal of Sol-Gel Science and Technology
74 rdf:type schema:Periodical
75 sg:person.0643673614.17 schema:affiliation https://www.grid.ac/institutes/grid.39679.32
76 schema:familyName Fuierer
77 schema:givenName Paul A.
78 schema:sameAs https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.0643673614.17
79 rdf:type schema:Person
80 sg:pub.10.1007/s10971-005-2521-8 schema:sameAs https://app.dimensions.ai/details/publication/pub.1028006782
81 https://doi.org/10.1007/s10971-005-2521-8
82 rdf:type schema:CreativeWork
83 sg:pub.10.1023/a:1015305328932 schema:sameAs https://app.dimensions.ai/details/publication/pub.1044107632
84 https://doi.org/10.1023/a:1015305328932
85 rdf:type schema:CreativeWork
86 sg:pub.10.1023/a:1018332221696 schema:sameAs https://app.dimensions.ai/details/publication/pub.1013824585
87 https://doi.org/10.1023/a:1018332221696
88 rdf:type schema:CreativeWork
89 sg:pub.10.1023/a:1023754718688 schema:sameAs https://app.dimensions.ai/details/publication/pub.1042932221
90 https://doi.org/10.1023/a:1023754718688
91 rdf:type schema:CreativeWork
92 sg:pub.10.1038/35104607 schema:sameAs https://app.dimensions.ai/details/publication/pub.1025421157
93 https://doi.org/10.1038/35104607
94 rdf:type schema:CreativeWork
95 sg:pub.10.1038/353737a0 schema:sameAs https://app.dimensions.ai/details/publication/pub.1014356537
96 https://doi.org/10.1038/353737a0
97 rdf:type schema:CreativeWork
98 https://doi.org/10.1006/jcat.2001.3316 schema:sameAs https://app.dimensions.ai/details/publication/pub.1032146733
99 rdf:type schema:CreativeWork
100 https://doi.org/10.1006/jcis.2002.8371 schema:sameAs https://app.dimensions.ai/details/publication/pub.1029059447
101 rdf:type schema:CreativeWork
102 https://doi.org/10.1016/0013-4686(82)80146-1 schema:sameAs https://app.dimensions.ai/details/publication/pub.1034171332
103 rdf:type schema:CreativeWork
104 https://doi.org/10.1016/0040-6090(94)06401-6 schema:sameAs https://app.dimensions.ai/details/publication/pub.1025109850
105 rdf:type schema:CreativeWork
106 https://doi.org/10.1016/0378-7753(85)88026-5 schema:sameAs https://app.dimensions.ai/details/publication/pub.1013387500
107 rdf:type schema:CreativeWork
108 https://doi.org/10.1021/ie0498551 schema:sameAs https://app.dimensions.ai/details/publication/pub.1055598639
109 rdf:type schema:CreativeWork
110 https://doi.org/10.1021/ja954172l schema:sameAs https://app.dimensions.ai/details/publication/pub.1055864300
111 rdf:type schema:CreativeWork
112 https://doi.org/10.1111/j.1151-2916.2000.tb01178.x schema:sameAs https://app.dimensions.ai/details/publication/pub.1018903570
113 rdf:type schema:CreativeWork
114 https://doi.org/10.1149/1.2048726 schema:sameAs https://app.dimensions.ai/details/publication/pub.1043058640
115 rdf:type schema:CreativeWork
116 https://www.grid.ac/institutes/grid.39679.32 schema:alternateName New Mexico Institute of Mining and Technology
117 schema:name Department of Materials Science and Engineering, New Mexico Institute of Mining and Technology, 801 Leroy Place, 87801, Socorro, NM
118 rdf:type schema:Organization
 




Preview window. Press ESC to close (or click here)


...