Speciation analysis of inorganic and organic arsenic in Canadian seafoods by chemical separation and neutron activation View Full Text


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Article Info

DATE

2018-10

AUTHORS

Y. Shi, A. Chatt

ABSTRACT

A new method consisting of methanol–methyl isobutyl ketone (MIBK)–water extraction and open-column cation exchange chromatography followed by HPLC was developed for the separation of total, residual, lipid-soluble, and five water soluble arsenic species including AsB, MMA, DMA, As(III), and As(V) in selected Canadian seafood samples. The mass fractions of arsenic were determined by neutron activation analysis with a detection limit of less than 20 µg kg−1. The method was validated by analyzing reference materials. The MIBK phase contained most of the lipid-soluble arsenic and indicated a linear relationship between the lipid content and lipid-soluble arsenic. More... »

PAGES

785-795

References to SciGraph publications

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    URI

    http://scigraph.springernature.com/pub.10.1007/s10967-018-6164-y

    DOI

    http://dx.doi.org/10.1007/s10967-018-6164-y

    DIMENSIONS

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