Radioanalytical separation and size-dependent ion exchange property of micelle-directed titanium phosphate nanocomposites View Full Text


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Article Info

DATE

2014-03

AUTHORS

Rajesh Chakraborty, Sriparna Chatterjee, Pabitra Chattopadhyay

ABSTRACT

Nanocomposite titanium-phosphate (TiP) of different sizes was synthesized using Triton X-100 (polyethylene glycol-p-isooctylphenyl ether) surfactant. The materials were characterized by FTIR and powdered X-ray diffraction (XRD). The structural and morphological details of the material were obtained by scanning electron microscopy (SEM) and transmission electron microscopy. The SEM study was followed by energy dispersive spectroscopic analysis for elemental analysis of the sample. The important peaks of the XRD spectra were analyzed to determine the probable composition of the material. The average size distribution of the particles was determined by dynamic light scattering method. Ion exchange capacity was measured for different metal ions with sizes of the TiP nanocomposite and size-dependent ion exchange property of the material was investigated thoroughly. The nanomaterial of the smallest size of around 43 nm was employed to separate carrier-free 137mBa from 137Cs in column chromatographic technique using 1.0 M HNO3 as eluting agent at pH 5. More... »

PAGES

1565-1570

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10967-013-2815-1

DOI

http://dx.doi.org/10.1007/s10967-013-2815-1

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1013202112


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