Neutron activation analysis of pure uranium: Preconcentration of impurity elements View Full Text


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Article Info

DATE

2009-06

AUTHORS

I. I. Sadikov, A. V. Rakhimov, M. I. Salimov, V. G. Zinov’ev, N. M. Mukhamedshina, F. A. Tashimova

ABSTRACT

We have developed a radiochemical neutron activation analysis technique (RNAA) of pure uranium with using extraction chromatographic separation of 239Np from impurity elements in TBP-6M HNO3 media. The estimation of influence of fission products of 235U on the results by radiochemical neutron activation analysis has been carried out. For it we have performed NAA with preconcentration of impurity elements. Experiments show that in this case the apparent concentration of Y, Zr, Mo, Cs, La, Ce, Pr, Nd exceeds the true concentration by 2500–3000 times. Therefore, determination of these elements is not possible by RNAA. This technique allowed to use the determination of 26 impurity elements with detection limit 10−5–10−9% by mass. This developed technique may be used for the determination of impurities in uranium and its compounds. More... »

PAGES

489-493

References to SciGraph publications

  • 2002-10. Elution of 235U fission products through a calcined hydrotalcite-packed column in JOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY
  • 2002-02. Separation of fission 99Mo from irradiated uranium using differential volatility in JOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY
  • 1986-09. Neutron activation analysis of PbxSn1-xTe using extraction chromatography in JOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY
  • 1993-03. Determination of impurities in nuclear fuel element components by neutron activation analysis in JOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY
  • 2002-02. Separation of fission 99Mo from irradiated uranium using differential volatility in JOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY
  • 2003-08. Separation of 132Te and 99Mo produced by 235U fission in JOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY
  • 1996-06. Determination of trace level impurities in uranium compounds by ICP-AES after organic extraction in ANALYTICAL AND BIOANALYTICAL CHEMISTRY
  • 1996-12. Instrumental neutron activation analysis for determining Mo in uranium containing materials in JOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY
  • 1995-12. Determination of traces of uranium in tungsten and molybdenum by radiochemical neutron activation analysis via the fission product140Ba in JOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY
  • 1983-03. Interference from uranium in neutron activation analysis or rare-earths in silicate rocks in JOURNAL OF RADIOANALYTICAL CHEMISTRY
  • 2001-04. Determination and evaluation of fission k0-factors for correctionof the 235U(n,f) interference in k0-NAA in JOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY
  • Identifiers

    URI

    http://scigraph.springernature.com/pub.10.1007/s10967-008-7389-y

    DOI

    http://dx.doi.org/10.1007/s10967-008-7389-y

    DIMENSIONS

    https://app.dimensions.ai/details/publication/pub.1045423137


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