A randomly branched poly(hydroxyl-β-amino amide): synthesis and complexation View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2010-11

AUTHORS

Chuan-bao Wu, Jian-yuan Hao, Xian-mo Deng

ABSTRACT

A novel type of polycation with high density of discrete charge, diversified amino group type and abundant hydrophilic short-chains was synthesized from tetraethylenepentamine (TEPA) and glycidol acrylate. The obtained polycation was abbreviated as PTGA. The structure and protonation property of PTGA was characterized by 1H NMR, FTIR, GPC and acid-base titration. 1H NMR of PTGA indicated that there were not only Michael addition and ring-opening but also high degree of amidation during polymerization. Only 12% ester group was left after polymerization. So PTGA is a kind of poly(hydroxyl-β-amino amide). Acid base titration indicated that the protonation of PTGA has wide protonation range and shows obvious proton sponge effect. The complexation of PTGA with polyanion was studied by using poly(acrylic acid) (PAA) as a model polyanion. The complex was characterized by dynamic light scattering and UV-Vis spectroscopy. It was found that the size of complex particle size first increased and then decreased as the charge ratio of PTGA to PAA. More... »

PAGES

869-876

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10965-009-9379-3

DOI

http://dx.doi.org/10.1007/s10965-009-9379-3

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1042223758


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