X-Ray Diffraction and Mössbauer Studies of Nanostructured Ni40Fe60 Powder: Structure Defects and Hyperfine Structure View Full Text


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Article Info

DATE

2022-09-02

AUTHORS

Nawel Khitouni, Wael Ben Mbarek, Abderrahim Guittoum, Joan Josep Suñol, Mohamed Khitouni, Meriem Azabou

ABSTRACT

A nanostructured nickel–iron alloy having the Ni40Fe60 composition was prepared through the mechanical alloying of the elemental powders in a high-energy ball mill P7 under an argon atmosphere. The microstructural, structure defects, and hyperfine properties during mechanical alloying were characterized by X-ray diffraction, scanning electron microscopy, and Mössbauer spectroscopy. The analysis of XRD spectra shows that the final product obtained was a nanostructured fcc-Ni(Fe)-rich phase. Whereas a more precise analysis by Mössbauer spectroscopy indicates that, in addition to paramagnetic phase rich with Ni, disordered ferromagnetic solid solutions fcc-Ni(Fe) and bcc-Fe(Ni) are present. The resulting nanostructure is demonstrated in accordance with the concept of dislocations; the dislocation densities were found to be around 5 × 1016 m−2 after 50 h milling. More... »

PAGES

3439-3446

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10948-022-06387-2

DOI

http://dx.doi.org/10.1007/s10948-022-06387-2

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1150719952


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