Triangular telluride complexes containing a cluster fragment [M3(µ3-Te)(µ2-Te2)3]4+ (M = Mo, W): Study of specific non-valence interactions View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2006-03

AUTHORS

A. V. Virovets, A. L. Gushchin, P. A. Abramov, N. I. Alferova, M. N. Sokolov, V. P. Fedin

ABSTRACT

Various synthetic approaches are used to obtain new triangular complexes with rare cluster nuclei M3Te74+ (M = Mo, W), as well as with partial substitution for chalcogen W3Te3.8Se3.24+. The crystalline structure has been identified for K5{[Mo3Te7(CN)6]2I}·2.5H2O (I), K3{[Mo3Te7(CN)6]SeCN}·3.25H2O (II), Cs2K{ [W3Te7(CN)6]Br0.8Cl0.2}·2.5H2O (III), Cs3{ [W3Te7(CN)6]Br}·2H2O (IV), Cs1.59K1.41{[W3Te3.8Se3.2× ×(CN)6]Br}·1,5H2O (V), [W3Te7((EtO)2PS2)3]Br (VI). The compounds are characterized by IR methods and electronic spectroscopy, electrospray-mass-spectrometry. The crystalline structure of this class of compounds is analyzed. Specific non-valence interactions in these systems are considered in detail. More... »

PAGES

326-338

References to SciGraph publications

  • 2003-09. The Coordination Polyhedra PdXn (X = Cl, Br, I) in Crystal Structures in RUSSIAN JOURNAL OF COORDINATION CHEMISTRY
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