Synthesis and crystal structure of KNa3[Fe3O(CH3COO)6(H2O)2]3 [α-P2W17Fe(H2O)O61]·32.5H2O View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2005-01

AUTHORS

N. V. Izarova, M. N. Sokolov, A. V. Virovets, H. G. Platas, V. P. Fedin

ABSTRACT

A complex of the composition KNa3[Fe3O(CH3COO)6(H2O)3]3 [α-P2W17Fe(H2O)O61]·32.5H2O (I) was obtained by interaction of FeCl3·6H2O and phosphotungstate K10[α2-P2W17O61]·20H2O in an acetate buffer with a yield of 52%. Compound I was characterized by single crystal X-ray phase analysis and IR spectroscopy. In the crystal structure, the Na and K cations bind [Fe3O(CH3COO)6(H2O)3]+ trinuclear cations and [α-P2W17Fe(H2O)O61]7− heteropolytungstate anions into infinite zigzag chains. More... »

PAGES

147-153

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10947-006-0021-5

DOI

http://dx.doi.org/10.1007/s10947-006-0021-5

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1042472314


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