Hydrothermal Synthesis, Crystal Structure and Magnetic Properties of Lithium Manganese Complex of Benzene-Hexacarboxylic Acid (Mellitic Acid) View Full Text


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Article Info

DATE

2010-09

AUTHORS

Guang-Xiang Liu, Heng Xu, Sadafumi Nishihara, Xiao-Ming Ren

ABSTRACT

A new mellitate complex LiMn[C6(COO)6]0.5(H2O)2 (1) has been synthesized by the reaction of mellitic acid and Mn(OAc)2·4H2O in the presence of LiOH·H2O. 1 was characterized by the elemental analyses, IR spectra, TGA and the single crystal X-ray diffraction. X-ray crystal structural analysis revealed that the Li cation has a distorted tetrahedral geometry, coordinated by three carboxylic oxygen atoms and one water molecule. The Mn cation is coordinated to one water molecule and five carboxylic oxygen atoms in a slightly distorted octahedral coordination geometry. The mellitate anions behave as a bridging ligand and link six lithium ions and eight manganese ions repeatedly to form an interesting three-dimensional metal–organic coordination polymer. Variable-temperature magnetic susceptibility measurements indicate the presence of antiferromagnetic behavior. A new mellitate complex LiMn[C6(COO)6]0.5(H2O)2 has been synthesized. X-ray crystal structural analysis revealed that the mellitate anions behave as the bridging ligand and link six lithium ions and eight manganese ions repeatedly to form an interesting three-dimensional metal–organic coordination polymer. Its magnetic behavior was studied. More... »

PAGES

564-569

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10904-010-9375-4

DOI

http://dx.doi.org/10.1007/s10904-010-9375-4

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1038444785


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