Syntheses and Characterizations of Three Cu(II) Complexes with 2,2′-Bipyridine-3,3′-dicarboxylate and N-Donor Ancillary Ligands View Full Text


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Article Info

DATE

2010-03

AUTHORS

Hong-Yu Xia, Guang-Xiang Liu, Sadafumi Nishihara, Yan Wang

ABSTRACT

Three novel inorganic–organic hybrid frameworks of [Cu(BPDC)(2,2′-bipy)] (1), [Cu(BPDC)(BIB)2·H2O]n (2) and [Cu(BPDC)(4,4′-bipy)]n (3) (BPDC2− = 2,2′-bipyridine-3,3′-dicarboxylate; 2,2′-bipy = 2,2′-bipyridine; BIB = 1,2-bis(imidazol-1-ylmethyl)benzene; 4,4′-bipy = 4,4′-bipyridine) were prepared. The three complexes have been characterized by the elemental analyses, IR spectra, TGA and the single crystal X-ray diffraction. Two intramolecular Cu(II) centers of 1 are encircled by two BPDC2− ligands forming an 18-membered ring, which is further assembled into a three-dimensional (3D) supramolecular architecture through the C–H···O hydrogen-bonding interactions. Complex 2 possesses a two-dimensional layer network, while complex 3 is a three-dimensional polymer composed of Cu-BPDC helical chains bridged by 4,4′-bipy. In addition, the electrochemistry of complex 1 was investigated. Syntheses and characterizations of three Cu(II) Complexes with 2,2′-bipyridine-3,3′-dicarboxylate and N-donor ancillary ligands. Three novel inorganic–organic hybrid frameworks have been characterized. Two intramolecular Cu(II) centers of 1 are encircled by two BPDC2− ligands forming an 18-membered ring, which is further assembled into a three-dimensional (3D) supramolecular architecture through the C–H···O hydrogen-bonding interactions. Complex 2 possesses a two-dimensional layer network, while complex 3 is a three-dimensional polymer composed of Cu-BPDC helical chains bridged by 4,4′-bipy. Hong-Yu Xia, Guang-Xiang Liu, Sadafumi Nishihara, Yan Wang More... »

PAGES

110-117

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10904-009-9306-4

DOI

http://dx.doi.org/10.1007/s10904-009-9306-4

DIMENSIONS

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