Chromo/Fluorogenic Detection of Co2+, Hg2+ and Cu2+ by the Simple Schiff Base Sensor View Full Text


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Article Info

DATE

2015-11-20

AUTHORS

Muhammad Saleem, Chung Ho Khang, Moon-Hwan kim, Ki Hwan Lee

ABSTRACT

Herein, we reported the ditriazole Schiff base derivative 1 and evaluated its photophysical properties on induction of varieties of metal ions including Na+, Ag+, Ni2+, Mn2+, Pd2+, Co2+, Hg2+, Cu2+, Pb2+, Cd2+, Zn2+, Sn2+, Fe2+, Fe3+, Cr3+ and Al3+, in order to figure out its potential as ion sensor. The ligand 1 exhibited the strong colorimetric change in the reaction solution as well as absorption spectral shifting with the concomitant appearance of well-defined isosbestic points only upon Co2+, Hg2+ and Cu2+ addition corroborates its applicability as multichannel ion detector. The different extent of spectral shifting as well as unique chromogenic change in the probe solution upon Co2+, Hg2+ and Cu2+ introduction can be used as the discrimination tool for these metal ions. The ligand-metal binding stoichiometry was assessed by their optical response which was further supported by the FT-IR, NMR and mass spectrometric analysis. The association constant and the detection limits of the ligand toward Co2+, Hg2+ and Cu2+ ions were calculated to be 1.52 × 10−8, 3.26 × 10−9, 1.16 × 10−8 and 3.87 × 10−10, 5.47 × 10−11, 8.91 × 10−11 M, respectively, employing the Benesi-Hilderbrand equation and 3 σ slope−1 methods. Furthermore, the successive addition of Co2+, Hg2+ and Cu2+ induce the constant decline in the fluorescence emission signal intensity of the probe. The quenching efficiency of the probe upon metallic induction was fitted to the Stern-Volmer equation which yielded the upward curvature in case of all the three metals ions (Co2+, Hg2+ and Cu2+) when (Io/I-1) was plotted against the quencher concentration indicating the occurrence of both the dynamic and static quenching process in the system with the average Stern-Volmer quenching constant values of 9.25 × 10−7, 1.14 × 10−7, 1.829 × 10−7, respectively. More... »

PAGES

11-22

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10895-015-1723-x

DOI

http://dx.doi.org/10.1007/s10895-015-1723-x

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1050505515

PUBMED

https://www.ncbi.nlm.nih.gov/pubmed/26585349


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