Bifunctional Calix[4]arene Sensor for Pb(II) and Cr2O72− Ions View Full Text


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Article Info

DATE

2013-03-06

AUTHORS

Mansoor Ahmed Qazi, Ümmühan Ocak, Miraç Ocak, Shahabuddin Memon, Imam Bakhsh Solangi

ABSTRACT

A readily available chromionophore 5,11,17,23-tetra-tert-butyl-25,27-bis(hydrazidecarbonylmethoxy)-26,28-dihydroxycalix[4]arene (HCC4) was employed as a chromogenic sensing probe selective for Pb(II) and Cr2O72− ions among a series of various ions such as Li(I), Na(I), K(I), Rb(I), Ba(II), Sr(II), Al(III), Cd(II), Co(II), Cu(II), Hg(II), Ni(II), Pb(II) and Zn(II) as well as Cr2O72−, CH3CO2−, Br−, Cl−, F−, I−, ClO4− and NO3− that have been examined by UV-visible and fluorescence spectroscopic techniques. The HCC4 in DCM-MeCN system forms 2:1 (ligand-metal) complex with Pb(II). It also shows 2:1 stoichiometry with Cr2O72−. The complexation phenomenon has been confirmed by FTIR spectroscopy that favors the selective nature of HCC4 with Pb(II) and Cr2O72−. Thermal gravimetric analysis (TGA) also supports its utility in drastic conditions. More... »

PAGES

575-590

References to SciGraph publications

  • 2003-04. Synthesis and Extraction Studies of a Versatile Calix[4]arene-Based “Proton-Switchable Extractant” for Toxic Metals and Dichromate Anions in JOURNAL OF INCLUSION PHENOMENA AND MACROCYCLIC CHEMISTRY
  • 2009-11-19. Convenient synthesis of tripodal-pyrrole receptor and anion binding properties in JOURNAL OF INCLUSION PHENOMENA AND MACROCYCLIC CHEMISTRY
  • 2007-07-18. A novel neutral receptor for selective recognition of H2PO4− in JOURNAL OF INCLUSION PHENOMENA AND MACROCYCLIC CHEMISTRY
  • 2011-01-08. Hg(II) Selective Complexation by Chromoionophoric Calix[4]arene Derivative in JOURNAL OF FLUORESCENCE
  • Identifiers

    URI

    http://scigraph.springernature.com/pub.10.1007/s10895-013-1200-3

    DOI

    http://dx.doi.org/10.1007/s10895-013-1200-3

    DIMENSIONS

    https://app.dimensions.ai/details/publication/pub.1024981657

    PUBMED

    https://www.ncbi.nlm.nih.gov/pubmed/23463295


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