Four Novel Coordination Polymers Based on Flexible 1,4-bis(1,2,4-triazol-1-ylmethyl)benzene Ligand: Synthesis, Structure, Luminescence and Magnetic Properties View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2019-03-27

AUTHORS

Xiaofei Xue, Yuqi Liu, Qiang Liu, Xinying Wang, Wei Li

ABSTRACT

Four new metal–organic coordination polymers, [Co5(btx)2(NDC)4(μ3-OH)2(H2O)2]·H2O}n(1), [Co(btx)(IP)]n(2), [Mn(btx)(NIP)(H2O)]n(3), {[Zn(btx)2(H2O)2]·2NO3·2H2O}n(4) (btx = 1,4-bis(1,2,4-triazol-1-ylmethyl)benzene; H2NDC = 1,4-naphthalenedicarboxylic acid; H2IP = 5-hydroxyisophthalic acid; H2NIP = 5-nitroisophthalic acid) were synthesized under hydrothermal conditions and characterized by techniques of single-crystal X-ray diffraction analysis, elemental analysis, infrared spectra (IR) and thermogravimetric analysis (TGA). The resulting MOFs analyses demonstrate that complex 1 displays a rare 3D 10-connected framework with the point symbol of {36·434·53·62} based on pentanuclear [Co5(μ3-OH)2(COO)8] cluster. Complex 2 presents a 5- connected 2D layer structure with the point symbol of {48·62}. Complex 3 features 4-connected threefold interpenetrating 3D network structure with the {65·8} point symbol. Complex 4 shows a 2D architecture. The variable-temperature magnetic susceptibility data show that the complex 1 exhibits antiferromagnetic interaction. Different to complex 1, the complex 2, 3 both show weak ferromagnetic interaction. Furthermore, the luminescence of complex 4 was also studied. More... »

PAGES

1-11

Identifiers

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http://scigraph.springernature.com/pub.10.1007/s10876-019-01539-2

DOI

http://dx.doi.org/10.1007/s10876-019-01539-2

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44 schema:description Four new metal–organic coordination polymers, [Co5(btx)2(NDC)4(μ3-OH)2(H2O)2]·H2O}n(1), [Co(btx)(IP)]n(2), [Mn(btx)(NIP)(H2O)]n(3), {[Zn(btx)2(H2O)2]·2NO3·2H2O}n(4) (btx = 1,4-bis(1,2,4-triazol-1-ylmethyl)benzene; H2NDC = 1,4-naphthalenedicarboxylic acid; H2IP = 5-hydroxyisophthalic acid; H2NIP = 5-nitroisophthalic acid) were synthesized under hydrothermal conditions and characterized by techniques of single-crystal X-ray diffraction analysis, elemental analysis, infrared spectra (IR) and thermogravimetric analysis (TGA). The resulting MOFs analyses demonstrate that complex 1 displays a rare 3D 10-connected framework with the point symbol of {36·434·53·62} based on pentanuclear [Co5(μ3-OH)2(COO)8] cluster. Complex 2 presents a 5- connected 2D layer structure with the point symbol of {48·62}. Complex 3 features 4-connected threefold interpenetrating 3D network structure with the {65·8} point symbol. Complex 4 shows a 2D architecture. The variable-temperature magnetic susceptibility data show that the complex 1 exhibits antiferromagnetic interaction. Different to complex 1, the complex 2, 3 both show weak ferromagnetic interaction. Furthermore, the luminescence of complex 4 was also studied.
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