[Ag7(H){S2CC(CN)2}6]6−: An Anionic Heptanuclear Silver Hydride Cluster Compound Stabilized by Dithiolate Ligands View Full Text


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Article Info

DATE

2019-03-28

AUTHORS

Ping-Kuei Liao, Kuan-Guan Liu, Ching-Shiang Fang, Ying-Yann Wu, C. W. Liu

ABSTRACT

In our attempts to identify probable intermediates in the preparation of anionic silver hydride cluster [Ag8(H){S2CC(CN)2}6]5− under the condition of excess NaBH4, we isolated and analyzed a new cluster compound, namely, [Bu4N]6[Ag7(H){S2CC(CN)2}6]. We report here the synthesis, crystal structure, characterizations by various spectroscopic (UV–Vis, IR, multinuclear NMR, elemental analyses) techniques and the luminescent properties of this cluster. Its X-ray crystal structure reveals that the cluster contains a distorted; tricapped tetrahedral silver core enclosed an interstitial hydride anion and is surrounded by six 1,1-dicyanoethylene-2,2-dithiolate ([S2CC(CN)2]2−, i-MNT) ligands. The presence of hydride inside the heptanuclear silver cluster is unequivocally certified by both 1H and 109Ag NMR spectroscopies. The title compound represents the first atomic precisely anionic Ag7-H skeleton with a non-disordered, tricapped tetrahedral silver framework. More... »

PAGES

1-9

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10876-019-01538-3

DOI

http://dx.doi.org/10.1007/s10876-019-01538-3

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https://app.dimensions.ai/details/publication/pub.1113051990


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