pH-Dependent Assembly of Three POM-Based Host–Guest Compounds Constituted by Keggin Polyoxoanions and 4,4′-Bipyridines View Full Text


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Article Info

DATE

2019-03

AUTHORS

Shu Y. Shi, Ling Y. Chen, Xun B. Zhao, Ying Li, Jun Zhang, Bai X. Ren, Xiao B. Cui

ABSTRACT

Three POM-based host–guest compounds constituted by Keggin-type polyoxometalates (POMs): (4,4′-Hbpy)3 [PMo12O40]·2H2O (1); (4,4′-H2bpy)3[PMo12O40]2·3H2O (2) and (4,4′-H2bpy) (4,4′-Hbpy)·[PW12O40]·4H2O (3) (bpy = 4,4′-bpyridine) have been synthesized hydrothermally and characterized by elemental analyses, IR, XPS spectra, powder XRD analyses, cyclic voltammetric measurements and single-crystal X-ray diffraction analyses. The three compounds all consist of Keggin-type POMs and 4,4′-bpy ligand, which are [PMo12O40]3− for 1–2 and [PW12O40]3− for 3. Through O···O interactions, Keggin POMs each other give rise to three different 3-D Supermolecular host structures, 4,4′-bpy and water molecules as guests accommodate different channels with H-bonding interactions. Discuss the pH role for the build POM based-hybrids contained 4,4′-bpy ligand. The photocatalytic properties of 1–3 have been investigated in the solid state. More... »

PAGES

299-310

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10876-018-1475-2

DOI

http://dx.doi.org/10.1007/s10876-018-1475-2

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1110707426


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Download the RDF metadata as:  json-ld nt turtle xml License info

HOW TO GET THIS DATA PROGRAMMATICALLY:

JSON-LD is a popular format for linked data which is fully compatible with JSON.

curl -H 'Accept: application/ld+json' 'https://scigraph.springernature.com/pub.10.1007/s10876-018-1475-2'

N-Triples is a line-based linked data format ideal for batch operations.

curl -H 'Accept: application/n-triples' 'https://scigraph.springernature.com/pub.10.1007/s10876-018-1475-2'

Turtle is a human-readable linked data format.

curl -H 'Accept: text/turtle' 'https://scigraph.springernature.com/pub.10.1007/s10876-018-1475-2'

RDF/XML is a standard XML format for linked data.

curl -H 'Accept: application/rdf+xml' 'https://scigraph.springernature.com/pub.10.1007/s10876-018-1475-2'


 

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