Decay of Hexaniobate Complexes of Mn(IV) and Pt(IV) in Alkaline Solutions: Some New Hexaniobate Salts View Full Text


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Article Info

DATE

2018-11

AUTHORS

Alexandra A. Shmakova, Rishat R. Shiriyazdanov, Albina R. Karimova, Nikolay B. Kompankov, Pavel A. Abramov, Maxim N. Sokolov

ABSTRACT

This research summarizes the behavior [Mn(Nb6O19)2]12− and [(Nb6O19)2(Pt(OH)2)2]12− in basic solutions at pH 12. After heating of [Mn(Nb6O19)2]12− for 20 min at 60° in the presence of NaOH new very unstable phase Na8[Nb6O19]·25H2O (1) was obtained. Gentle (60 °C) heating of a solution of [(Nb6O19)2(Pt(OH)2)2]12− for 10 min in the presence of NaOH causes rearrangement into [Pt(Nb6O19)2]12−, which was isolated as Na12[Pt(Nb6O19)2]·52H2O (2). Longer heating yields white insoluble amorphous precipitate and crystals of a new hexaniobate phase K5Na3[Nb6O19]·9H2O (3). Crystal structures of the products and their structural relationship with known analogs are discussed. More... »

PAGES

1201-1207

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10876-018-1439-6

DOI

http://dx.doi.org/10.1007/s10876-018-1439-6

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1106014367


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46 schema:description This research summarizes the behavior [Mn(Nb6O19)2]12− and [(Nb6O19)2(Pt(OH)2)2]12− in basic solutions at pH 12. After heating of [Mn(Nb6O19)2]12− for 20 min at 60° in the presence of NaOH new very unstable phase Na8[Nb6O19]·25H2O (1) was obtained. Gentle (60 °C) heating of a solution of [(Nb6O19)2(Pt(OH)2)2]12− for 10 min in the presence of NaOH causes rearrangement into [Pt(Nb6O19)2]12−, which was isolated as Na12[Pt(Nb6O19)2]·52H2O (2). Longer heating yields white insoluble amorphous precipitate and crystals of a new hexaniobate phase K5Na3[Nb6O19]·9H2O (3). Crystal structures of the products and their structural relationship with known analogs are discussed.
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