Supramolecular Adduct of γ-Cyclodextrin and [{Re6Q8}(H2O)6]2+ (Q=S, Se) View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2018-01

AUTHORS

Pavel A. Abramov, Anton A. Ivanov, Michael A. Shestopalov, Mhamad A. Moussawi, Emmanuel Cadot, Sébastien Floquet, Mohamed Haouas, Maxim N. Sokolov

ABSTRACT

Slow evaporation of water solution of [{Re6S8}(H2O)6]2+ generated in situ from [{Re6S8}(OH)6]4– in presence of γ-cyclodextrin (CD) leads to crystallization of {[{Re6S8}(H2O)6] ⊂ [γ-CD]}(NO3)2·12H2O (1·12H2O) supramolecular complex, which was characterized by single-crystal X-ray diffraction crystallography, IR-spectroscopy, thermogravimetric and elemental analyses. X-ray analysis confirms the formation of 1:1 {[{Re6S8}(H2O)6] ⊂ [γ-CD]}2+ inclusion compound in the solid state. However, no adduct formation was detected between [{Re6S8}(H2O)6]2+ and γ-cyclodextrin in solution, according to 1H NMR spectroscopy. In the case of in situ generated [{Re6Se8}(H2O)6]2+ the reaction solution with γ-cyclodextrin is unstable and during the crystallization only amorphous precipitate has been obtained. More... »

PAGES

9-13

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10876-017-1312-z

DOI

http://dx.doi.org/10.1007/s10876-017-1312-z

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1092500857


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36 schema:description Slow evaporation of water solution of [{Re6S8}(H2O)6]2+ generated in situ from [{Re6S8}(OH)6]4– in presence of γ-cyclodextrin (CD) leads to crystallization of {[{Re6S8}(H2O)6] ⊂ [γ-CD]}(NO3)2·12H2O (1·12H2O) supramolecular complex, which was characterized by single-crystal X-ray diffraction crystallography, IR-spectroscopy, thermogravimetric and elemental analyses. X-ray analysis confirms the formation of 1:1 {[{Re6S8}(H2O)6] ⊂ [γ-CD]}2+ inclusion compound in the solid state. However, no adduct formation was detected between [{Re6S8}(H2O)6]2+ and γ-cyclodextrin in solution, according to 1H NMR spectroscopy. In the case of in situ generated [{Re6Se8}(H2O)6]2+ the reaction solution with γ-cyclodextrin is unstable and during the crystallization only amorphous precipitate has been obtained.
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