Crystal Structure of Cs4[{(C6H6)Ru}2Nb6O19]·8MeOH·2H2O. Structural Overview of Hybrid Organometallic Hexametalates of Niobium and Tantalum: Alkali Metal Coordination Behavior View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2017-03

AUTHORS

Pavel A. Abramov, Tatiana P. Zemerova, Maxim N. Sokolov

ABSTRACT

Reaction of Cs8[Nb6O19]·14H2O with [(C6H6)RuCl2]2 leads to the formation of trans-[{(C6H6)Ru}2Nb6O19]4− (1). Evaporation of the reaction solution and extraction into methanol (MeOH) yielded Cs4[{(C6H6)Ru}2Nb6O19]·8MeOH·2H2O (1a) as main product together with a small amount of Cs4[{(C6H6)Ru}2Nb6O19]·4MeOH·6H2O (1b), both characterized by X-ray analysis. These structures complete a set of known organometallic polyoxoniobate or polyoxotantalate complexes [{Cp*M′}xM6O19]n− and [{(C6H6)Ru}xM6O19]n− (M = Nb, Ta; M′ = Rh, Ir; x = 1, 2; n = 6, 4; Cp* = η5-C5(CH3)5) and give additional information about the importance of cation–anion interactions in the crystal structures of such complexes. More... »

PAGES

725-734

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10876-016-1116-6

DOI

http://dx.doi.org/10.1007/s10876-016-1116-6

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https://app.dimensions.ai/details/publication/pub.1036427969


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136 https://www.grid.ac/institutes/grid.77268.3c schema:alternateName Kazan Federal University
137 schema:name Kazan Federal University, 18 ul. Kremlyovskaya, 420008, Kazan, Russia
138 Nikolaev Institute of Inorganic Chemistry SB RAS, 3 Akad. Lavrentieva Ave, 630090, Novosibirsk, Russia
139 Novosibirsk State University, ul. Pirogova 2, 630090, Novosibirsk, Russia
140 rdf:type schema:Organization
 




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