1,1-Cyclohexanediacetate as New Bridging Ligand for Assembling of Homo- and Heterometallic Molecular Complexes with Cu3II, Cu2IILn2III (Ln = Sm or ... View Full Text


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Article Info

DATE

2014-06-08

AUTHORS

Natalya Gogoleva, Ekaterina Zorina-Tikhonova, Grigory Aleksandrov, Anatoly Lermontov, Nikolay Efimov, Artem Bogomyakov, Elena Ugolkova, Sergey Kolotilov, Aleksey Sidorov, Vadim Minin, Vladimir Novotortsev, Igor Eremenko

ABSTRACT

Interaction of [Cu2(Piv)4(HPiv)2] (Piv− = pivalate) with tetrabutylammonium salt of 1,1-cyclohexanediacetate (Chda2−) and 2,2-bipyridine (2,2′-bpy) in acetonitrile led to formation of the trinuclear homometallic complex [Cu3(2,2′-bpy)2(Chda)2(Piv)2]·2MeCN·0.4H2O (1·2MeCN·0.4H2O). In similar conditions but in presence of [Ln2(Piv)6(HPiv)7] tetranuclear heterometallic complexes [Ln2IIICu2II(2,2′-bpy)2(Chda)2(Piv)6] (Ln = SmIII, 2·2MeCN, or GdIII, 3·2MeCN·5H2O) and [Gd2IIINi2II(2,2′-bpy)2(Chda)2(Piv)6] (4) were synthesized. Carboxylic groups in Piv− and Chda2− act as bridges between the metal ions in all complexes. Temperature dependencies of magnetic susceptibilities and room-temperature solid-state ESR spectra of compounds 2·2MeCN, 3·2MeCN·5H2O, 4 were studied and analyzed. More... »

PAGES

137-155

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10876-014-0740-2

DOI

http://dx.doi.org/10.1007/s10876-014-0740-2

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1000871830


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