Novel Three-Dimensional Coordination Polymers Based on [Mo6Se8(CN)6]7− Anions and Mn2+ Cations View Full Text


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Article Info

DATE

2009-03

AUTHORS

Konstantin A. Brylev, Nikolay G. Naumov, Alexander V. Virovets, Sung-Jin Kim, Vladimir E. Fedorov

ABSTRACT

Three novel coordination polymers K5[MnMo6Se8(CN)6] · 8H2O (1), (Me4N)4[{Mn(H2O)2}1.5Mo6Se8(CN)6] · 4H2O (2), and K3[{Mn2(H2O)4}Mo6Se8(CN)6] · 7H2O (3) have been synthesized by layering of a methanol solution of [Mn(salen)]CH3COO (salen–N,N′-bis(salicylidene)ethylenediamine) on an aqueous solution of K7[Mo6Se8(CN)6] · 8H2O. The compounds have been characterized by single-crystal X-ray diffraction analysis. All structures are based on negatively charged porous polymer frameworks where CN groups of [Mo6Se8(CN)6]7− cluster complexes are coordinated to Mn2+ cations. Cavities in the frameworks are filled by additional cations and solvate water molecules. More... »

PAGES

165-176

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10876-008-0215-4

DOI

http://dx.doi.org/10.1007/s10876-008-0215-4

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1021794572


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