Synthesis, Spectroscopic and Thermal Studies of Zinc(II) Complexes with the Symmetrical Bidentate Schiff-Base Ligand (2,3-MeO-ba)2en: Crystal Structure of Zn((2,3-MeO-ba)2en)I2 View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2012-01

AUTHORS

Aliakbar Dehno Khalaji, Gholamhossein Grivani, Samaneh Jalali Akerdi, Helen Stoeckli-Evans, Debasis Das

ABSTRACT

Two zinc(II) complexes [ZnI2((2,3-MeO-ba)2en)] (1) and [ZnCl2((2,3-MeO-ba)2en)] (2), with the symmetrical bidentate Schiff-base ligand (2,3-MeO-ba)2en [N,N′-bis(2,3-dimethoxybenzylidene)-1,2-diaminoethane] have been synthesized and characterized by elemental analyses (CHN), FT-IR and 1H-NMR spectroscopy. The thermal behaviors of these complexes were studied using thermogravimetry in order to evaluate their thermal stability and thermal decomposition pathways. The crystal structure of [ZnI2((2,3-MeO-ba)2en)] (1) was determined from single-crystal X-ray diffraction. The coordination polyhedron about the zinc(II) center in the complex 1 is best described as a distorted tetrahedron. Zinc(II) complexes [ZnX2((2,3-MeO-ba)2en)] (X = I (1) and Cl (2)) have been synthesized and characterized by elemental analyses (CHN), FT-IR and 1H-NMR spectroscopy. The crystal structure of 1 was determined from single-crystal X-ray diffraction. The coordination polyhedron about the zinc(II) center in the complex 1 is best described as a distorted tetrahedron. More... »

PAGES

83-88

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10870-011-0207-3

DOI

http://dx.doi.org/10.1007/s10870-011-0207-3

DIMENSIONS

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