Synthesis, Crystal Structure, Electronic Absorption and Magnetic Properties of a Novel Anion-Radical Salt Based on 7,7,8,8-Tetracyanoquinodimethane View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2011-09

AUTHORS

Guang-Xiang Liu, Wei Guo, Hao Yang, Sadafumi Nishihara, Xiao-Ming Ren

ABSTRACT

A novel anion-radical salt, (AP)(TCNQ)·H2O (1), where AP = 4-amino-1-butylpyridin-1-ium and TCNQ = 7,7,8,8-tetracyanoquinodimethane, has been synthesized. X-ray single crystal structural analyses show that the TCNQ anions and AP cations form a well-separated stacking column. The TCNQ anions are uniformly spaced to give a one-dimensional (1-D) chain structure through π···π interactions, which is rarely observed in TCNQ anion-radical system. It is noteworthy that compound 1 shows a peculiar magnetic transition from paramagnetism in the high-temperature (HT) phase to spin gap in low-temperature (LT) phase. A novel anion-radical salt, (AP)(TCNQ)•H2O (1), has been synthesized. X-ray single crystal structural analyses show that the TCNQ anions and AP cations form a well-separated stacking column. The TCNQ anions are uniformly spaced to give a one-dimensional (1-D) chain structure through π···π interactions, which is rarely observed in TCNQ anion-radical system. More... »

PAGES

1262

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10870-011-0085-8

DOI

http://dx.doi.org/10.1007/s10870-011-0085-8

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https://app.dimensions.ai/details/publication/pub.1017931147


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