Isolation and Crystal Structure Determination of 3,5,4′-Trihydroxy-6,7-Dimethoxy-Flavone (Eupalitin) from Asparagus falcatus (Linn.) View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2010-06

AUTHORS

Raza Murad Ghalib, Sayed Hasan Mehdi, Rokiah Hashim, Othman Sulaiman, Arto Valkonen, Kari Rissanen, Srećko R. Trifunović

ABSTRACT

In this paper the title compound 3,5,4′-trihydroxy-6,7-dimethoxy-flavone (Eupalitin) has been isolated from Asparagus falcatus and characterized by UV, IR, NMR, mass spectra and X-ray single crystal diffraction. The 3,5,4′-trihydroxy-6,7-dimethoxy-flavone crystallizes in a monoclinic space group P21/n with a = 6.2527(2), b = 17.2821(6), c = 13.5476(5) Å, β = 100.274(2)° and Z = 4, β = 100.274(2)° and V = 1440.48(9) Å3. The crystal structure are stabilized by intra- and intermolecular O–H···O hydrogen bonds. Molecules pack into infinite zigzag-like layers with these hydrogen bonds. The title compound 3,5,4′-trihydroxy-6,7-dimethoxy-flavone (Eupalitin) has been isolated from Asparagus falcatus and characterized by UV, IR, NMR, mass spectra and X-ray single crystal diffraction. More... »

PAGES

510-513

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10870-010-9687-9

DOI

http://dx.doi.org/10.1007/s10870-010-9687-9

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https://app.dimensions.ai/details/publication/pub.1009444396


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