α-Diimine Chelation at a Triosmium Cluster: Synthesis and X-ray Structure of 1,1-Os3(CO)9(μ-CO)(1,10-phen) View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2007-09

AUTHORS

Bhaskar Poola, Xiaoping Wang, Michael G. Richmond

ABSTRACT

The α-diimine ligand 1,10-phenanthroline (phen) reacts with the activated cluster 1,2-Os3(CO)10(MeCN)2 to afford the carbonyl-bridged cluster 1,1-Os3(CO)9(μ-CO)(phen), which has been characterized by IR and NMR spectroscopies and X-ray diffraction analysis. Replacement of the 1,5-cyclooctadiene (cod) ligand in 1,1-Os3(CO)10(cod) by phen proceeds sluggishly over a 24 h period, showing less than 5% conversion to 1,1-Os3(CO)9(μ-CO)(phen). α-Diimine Chelation at a Triosmium Cluster: Synthesis and X-ray Structure of 1,1-Os3(CO)9(μ-CO)(1,10-phen) Bhaskar Poola, Xiaoping Wang, and Michael G. Richmond The reaction between the triosmium cluster 1,2-Os3(CO)10(MeCN)2 and 1,10-phenanthroline yields 1,1-Os3(CO)9(μ-CO)(phen) at room temperature. The presence of a bridging carbonyl group in the product cluster has been observed by IR spectroscopy and confirmed by X-ray crystallography. More... »

PAGES

641-644

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10870-007-9225-6

DOI

http://dx.doi.org/10.1007/s10870-007-9225-6

DIMENSIONS

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