Ontology type: schema:ScholarlyArticle
2018-12
AUTHORSThomas Wiegand, Andreas Hunkeler, Alexander Däpp, Joeri Verasdonck, Riccardo Cadalbert, Luc Bousset, Ronald Melki, Anja Böckmann, Beat H. Meier
ABSTRACTMagic-angle spinning (MAS) is mandatory in solid-state NMR experiments to achieve resolved spectra. In rare cases, instabilities in the rotation or damage of either the rotor or the rotor cap can lead to a so called "rotor crash" involving a disintegration of the sample container and possibly the release of an aerosol or of dust. We present a modified design of a 3.2 mm probe with a confining chamber which in case of a rotor crash prevents the release of aerosols and possibly hazardous materials. 1D and 2D NMR experiments show that such a hazardous material-confining MAS probe ("CONFINE-MAS" probe) has a similar sensitivity compared to a standard probe and performs equally well in terms of spinning stability. We illustrate the CONFINE-MAS probe properties and performance by application to a fungal amyloid. More... »
PAGES171-177
http://scigraph.springernature.com/pub.10.1007/s10858-018-0218-x
DOIhttp://dx.doi.org/10.1007/s10858-018-0218-x
DIMENSIONShttps://app.dimensions.ai/details/publication/pub.1110487089
PUBMEDhttps://www.ncbi.nlm.nih.gov/pubmed/30536187
JSON-LD is the canonical representation for SciGraph data.
TIP: You can open this SciGraph record using an external JSON-LD service: JSON-LD Playground Google SDTT
[
{
"@context": "https://springernature.github.io/scigraph/jsonld/sgcontext.json",
"about": [
{
"id": "http://purl.org/au-research/vocabulary/anzsrc-for/2008/0306",
"inDefinedTermSet": "http://purl.org/au-research/vocabulary/anzsrc-for/2008/",
"name": "Physical Chemistry (incl. Structural)",
"type": "DefinedTerm"
},
{
"id": "http://purl.org/au-research/vocabulary/anzsrc-for/2008/03",
"inDefinedTermSet": "http://purl.org/au-research/vocabulary/anzsrc-for/2008/",
"name": "Chemical Sciences",
"type": "DefinedTerm"
}
],
"author": [
{
"affiliation": {
"alternateName": "Swiss Federal Institute of Technology in Zurich",
"id": "https://www.grid.ac/institutes/grid.5801.c",
"name": [
"Physical Chemistry, ETH Z\u00fcrich, Vladimir-Prelog-Weg 2, 8093, Z\u00fcrich, Switzerland"
],
"type": "Organization"
},
"familyName": "Wiegand",
"givenName": "Thomas",
"id": "sg:person.0627204513.50",
"sameAs": [
"https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.0627204513.50"
],
"type": "Person"
},
{
"affiliation": {
"alternateName": "Swiss Federal Institute of Technology in Zurich",
"id": "https://www.grid.ac/institutes/grid.5801.c",
"name": [
"Physical Chemistry, ETH Z\u00fcrich, Vladimir-Prelog-Weg 2, 8093, Z\u00fcrich, Switzerland"
],
"type": "Organization"
},
"familyName": "Hunkeler",
"givenName": "Andreas",
"id": "sg:person.01074243371.48",
"sameAs": [
"https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.01074243371.48"
],
"type": "Person"
},
{
"affiliation": {
"alternateName": "Swiss Federal Institute of Technology in Zurich",
"id": "https://www.grid.ac/institutes/grid.5801.c",
"name": [
"Physical Chemistry, ETH Z\u00fcrich, Vladimir-Prelog-Weg 2, 8093, Z\u00fcrich, Switzerland"
],
"type": "Organization"
},
"familyName": "D\u00e4pp",
"givenName": "Alexander",
"id": "sg:person.01002477547.09",
"sameAs": [
"https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.01002477547.09"
],
"type": "Person"
},
{
"affiliation": {
"alternateName": "Swiss Federal Institute of Technology in Zurich",
"id": "https://www.grid.ac/institutes/grid.5801.c",
"name": [
"Physical Chemistry, ETH Z\u00fcrich, Vladimir-Prelog-Weg 2, 8093, Z\u00fcrich, Switzerland"
],
"type": "Organization"
},
"familyName": "Verasdonck",
"givenName": "Joeri",
"id": "sg:person.0666573043.52",
"sameAs": [
"https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.0666573043.52"
],
"type": "Person"
},
{
"affiliation": {
"alternateName": "Swiss Federal Institute of Technology in Zurich",
"id": "https://www.grid.ac/institutes/grid.5801.c",
"name": [
"Physical Chemistry, ETH Z\u00fcrich, Vladimir-Prelog-Weg 2, 8093, Z\u00fcrich, Switzerland"
],
"type": "Organization"
},
"familyName": "Cadalbert",
"givenName": "Riccardo",
"id": "sg:person.01161224413.59",
"sameAs": [
"https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.01161224413.59"
],
"type": "Person"
},
{
"affiliation": {
"alternateName": "Institut d'Imagerie Biom\u00e9dicale",
"id": "https://www.grid.ac/institutes/grid.457286.a",
"name": [
"Institut Fran\u00e7ois Jacob, MIRCen, CEA, Laboratory of Neurodegenerative Diseases, CNRS, 18 Rue du Panorama, 92265, Fontenay-aux-Roses, France"
],
"type": "Organization"
},
"familyName": "Bousset",
"givenName": "Luc",
"id": "sg:person.01303024074.26",
"sameAs": [
"https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.01303024074.26"
],
"type": "Person"
},
{
"affiliation": {
"alternateName": "Institut d'Imagerie Biom\u00e9dicale",
"id": "https://www.grid.ac/institutes/grid.457286.a",
"name": [
"Institut Fran\u00e7ois Jacob, MIRCen, CEA, Laboratory of Neurodegenerative Diseases, CNRS, 18 Rue du Panorama, 92265, Fontenay-aux-Roses, France"
],
"type": "Organization"
},
"familyName": "Melki",
"givenName": "Ronald",
"id": "sg:person.01224221363.53",
"sameAs": [
"https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.01224221363.53"
],
"type": "Person"
},
{
"affiliation": {
"alternateName": "University of Lyon System",
"id": "https://www.grid.ac/institutes/grid.25697.3f",
"name": [
"Molecular Microbiology and Structural Biochemistry, UMR 5086 CNRS, Universit\u00e9 de Lyon, Labex Ecofect, 69367, Lyon, France"
],
"type": "Organization"
},
"familyName": "B\u00f6ckmann",
"givenName": "Anja",
"id": "sg:person.01202540744.82",
"sameAs": [
"https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.01202540744.82"
],
"type": "Person"
},
{
"affiliation": {
"alternateName": "Swiss Federal Institute of Technology in Zurich",
"id": "https://www.grid.ac/institutes/grid.5801.c",
"name": [
"Physical Chemistry, ETH Z\u00fcrich, Vladimir-Prelog-Weg 2, 8093, Z\u00fcrich, Switzerland"
],
"type": "Organization"
},
"familyName": "Meier",
"givenName": "Beat H.",
"id": "sg:person.0621622733.90",
"sameAs": [
"https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.0621622733.90"
],
"type": "Person"
}
],
"citation": [
{
"id": "https://doi.org/10.1016/j.jmr.2015.01.012",
"sameAs": [
"https://app.dimensions.ai/details/publication/pub.1008633378"
],
"type": "CreativeWork"
},
{
"id": "sg:pub.10.1038/nsb0602-416",
"sameAs": [
"https://app.dimensions.ai/details/publication/pub.1012061819",
"https://doi.org/10.1038/nsb0602-416"
],
"type": "CreativeWork"
},
{
"id": "sg:pub.10.1007/s10858-011-9569-2",
"sameAs": [
"https://app.dimensions.ai/details/publication/pub.1013434278",
"https://doi.org/10.1007/s10858-011-9569-2"
],
"type": "CreativeWork"
},
{
"id": "sg:pub.10.1038/nsmb.3194",
"sameAs": [
"https://app.dimensions.ai/details/publication/pub.1016142352",
"https://doi.org/10.1038/nsmb.3194"
],
"type": "CreativeWork"
},
{
"id": "https://doi.org/10.1002/anie.201408598",
"sameAs": [
"https://app.dimensions.ai/details/publication/pub.1023290329"
],
"type": "CreativeWork"
},
{
"id": "https://doi.org/10.1002/prot.20449",
"sameAs": [
"https://app.dimensions.ai/details/publication/pub.1027764068"
],
"type": "CreativeWork"
},
{
"id": "https://doi.org/10.1073/pnas.1600749113",
"sameAs": [
"https://app.dimensions.ai/details/publication/pub.1032221293"
],
"type": "CreativeWork"
},
{
"id": "sg:pub.10.1007/s10858-009-9374-3",
"sameAs": [
"https://app.dimensions.ai/details/publication/pub.1033669162",
"https://doi.org/10.1007/s10858-009-9374-3"
],
"type": "CreativeWork"
},
{
"id": "sg:pub.10.1007/s10858-009-9374-3",
"sameAs": [
"https://app.dimensions.ai/details/publication/pub.1033669162",
"https://doi.org/10.1007/s10858-009-9374-3"
],
"type": "CreativeWork"
},
{
"id": "https://doi.org/10.1080/00268979809483251",
"sameAs": [
"https://app.dimensions.ai/details/publication/pub.1038463620"
],
"type": "CreativeWork"
},
{
"id": "https://doi.org/10.3233/jpd-150691",
"sameAs": [
"https://app.dimensions.ai/details/publication/pub.1041954984"
],
"type": "CreativeWork"
},
{
"id": "https://doi.org/10.1016/s0009-2614(01)00791-6",
"sameAs": [
"https://app.dimensions.ai/details/publication/pub.1047325943"
],
"type": "CreativeWork"
},
{
"id": "https://doi.org/10.1016/j.jmr.2007.09.008",
"sameAs": [
"https://app.dimensions.ai/details/publication/pub.1052702355"
],
"type": "CreativeWork"
},
{
"id": "sg:pub.10.1038/1821659a0",
"sameAs": [
"https://app.dimensions.ai/details/publication/pub.1053527752",
"https://doi.org/10.1038/1821659a0"
],
"type": "CreativeWork"
},
{
"id": "https://doi.org/10.1016/s0009-2614(99)00533-3",
"sameAs": [
"https://app.dimensions.ai/details/publication/pub.1053563394"
],
"type": "CreativeWork"
},
{
"id": "https://doi.org/10.1021/ja104213j",
"sameAs": [
"https://app.dimensions.ai/details/publication/pub.1055847672"
],
"type": "CreativeWork"
},
{
"id": "https://doi.org/10.1021/ja104213j",
"sameAs": [
"https://app.dimensions.ai/details/publication/pub.1055847672"
],
"type": "CreativeWork"
},
{
"id": "https://doi.org/10.1103/physrevlett.2.285",
"sameAs": [
"https://app.dimensions.ai/details/publication/pub.1060770662"
],
"type": "CreativeWork"
},
{
"id": "https://doi.org/10.1103/physrevlett.2.285",
"sameAs": [
"https://app.dimensions.ai/details/publication/pub.1060770662"
],
"type": "CreativeWork"
},
{
"id": "https://doi.org/10.1126/science.1151839",
"sameAs": [
"https://app.dimensions.ai/details/publication/pub.1062457243"
],
"type": "CreativeWork"
},
{
"id": "https://doi.org/10.1177/109135059800300111",
"sameAs": [
"https://app.dimensions.ai/details/publication/pub.1063976419"
],
"type": "CreativeWork"
},
{
"id": "https://doi.org/10.1177/109135059800300111",
"sameAs": [
"https://app.dimensions.ai/details/publication/pub.1063976419"
],
"type": "CreativeWork"
}
],
"datePublished": "2018-12",
"datePublishedReg": "2018-12-01",
"description": "Magic-angle spinning (MAS) is mandatory in solid-state NMR experiments to achieve resolved spectra. In rare cases, instabilities in the rotation or damage of either the rotor or the rotor cap can lead to a so called \"rotor crash\" involving a disintegration of the sample container and possibly the release of an aerosol or of dust. We present a modified design of a 3.2\u00a0mm probe with a confining chamber which in case of a rotor crash prevents the release of aerosols and possibly hazardous materials. 1D and 2D NMR experiments show that such a hazardous material-confining MAS probe (\"CONFINE-MAS\" probe) has a similar sensitivity compared to a standard probe and performs equally well in terms of spinning stability. We illustrate the CONFINE-MAS probe properties and performance by application to a fungal amyloid.",
"genre": "research_article",
"id": "sg:pub.10.1007/s10858-018-0218-x",
"inLanguage": [
"en"
],
"isAccessibleForFree": false,
"isFundedItemOf": [
{
"id": "sg:grant.5180950",
"type": "MonetaryGrant"
},
{
"id": "sg:grant.6814619",
"type": "MonetaryGrant"
}
],
"isPartOf": [
{
"id": "sg:journal.1101518",
"issn": [
"0925-2738",
"1573-5001"
],
"name": "Journal of Biomolecular NMR",
"type": "Periodical"
},
{
"issueNumber": "3-4",
"type": "PublicationIssue"
},
{
"type": "PublicationVolume",
"volumeNumber": "72"
}
],
"name": "CONFINE-MAS: a magic-angle spinning NMR probe that confines the sample in case of a rotor explosion",
"pagination": "171-177",
"productId": [
{
"name": "readcube_id",
"type": "PropertyValue",
"value": [
"8f10a27dac32d7125ccda12c1c26cb759dc06a843e28c98cb7a955f0bd505a2a"
]
},
{
"name": "pubmed_id",
"type": "PropertyValue",
"value": [
"30536187"
]
},
{
"name": "nlm_unique_id",
"type": "PropertyValue",
"value": [
"9110829"
]
},
{
"name": "doi",
"type": "PropertyValue",
"value": [
"10.1007/s10858-018-0218-x"
]
},
{
"name": "dimensions_id",
"type": "PropertyValue",
"value": [
"pub.1110487089"
]
}
],
"sameAs": [
"https://doi.org/10.1007/s10858-018-0218-x",
"https://app.dimensions.ai/details/publication/pub.1110487089"
],
"sdDataset": "articles",
"sdDatePublished": "2019-04-11T08:31",
"sdLicense": "https://scigraph.springernature.com/explorer/license/",
"sdPublisher": {
"name": "Springer Nature - SN SciGraph project",
"type": "Organization"
},
"sdSource": "s3://com-uberresearch-data-dimensions-target-20181106-alternative/cleanup/v134/2549eaecd7973599484d7c17b260dba0a4ecb94b/merge/v9/a6c9fde33151104705d4d7ff012ea9563521a3ce/jats-lookup/v90/0000000309_0000000309/records_106277_00000000.jsonl",
"type": "ScholarlyArticle",
"url": "https://link.springer.com/10.1007%2Fs10858-018-0218-x"
}
]Download the RDF metadata as: json-ld nt turtle xml License info
JSON-LD is a popular format for linked data which is fully compatible with JSON.
curl -H 'Accept: application/ld+json' 'https://scigraph.springernature.com/pub.10.1007/s10858-018-0218-x'
N-Triples is a line-based linked data format ideal for batch operations.
curl -H 'Accept: application/n-triples' 'https://scigraph.springernature.com/pub.10.1007/s10858-018-0218-x'
Turtle is a human-readable linked data format.
curl -H 'Accept: text/turtle' 'https://scigraph.springernature.com/pub.10.1007/s10858-018-0218-x'
RDF/XML is a standard XML format for linked data.
curl -H 'Accept: application/rdf+xml' 'https://scigraph.springernature.com/pub.10.1007/s10858-018-0218-x'
This table displays all metadata directly associated to this object as RDF triples.
194 TRIPLES
21 PREDICATES
47 URIs
21 LITERALS
9 BLANK NODES