CONFINE-MAS: a magic-angle spinning NMR probe that confines the sample in case of a rotor explosion View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2018-12

AUTHORS

Thomas Wiegand, Andreas Hunkeler, Alexander Däpp, Joeri Verasdonck, Riccardo Cadalbert, Luc Bousset, Ronald Melki, Anja Böckmann, Beat H. Meier

ABSTRACT

Magic-angle spinning (MAS) is mandatory in solid-state NMR experiments to achieve resolved spectra. In rare cases, instabilities in the rotation or damage of either the rotor or the rotor cap can lead to a so called "rotor crash" involving a disintegration of the sample container and possibly the release of an aerosol or of dust. We present a modified design of a 3.2 mm probe with a confining chamber which in case of a rotor crash prevents the release of aerosols and possibly hazardous materials. 1D and 2D NMR experiments show that such a hazardous material-confining MAS probe ("CONFINE-MAS" probe) has a similar sensitivity compared to a standard probe and performs equally well in terms of spinning stability. We illustrate the CONFINE-MAS probe properties and performance by application to a fungal amyloid. More... »

PAGES

171-177

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10858-018-0218-x

DOI

http://dx.doi.org/10.1007/s10858-018-0218-x

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1110487089

PUBMED

https://www.ncbi.nlm.nih.gov/pubmed/30536187


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