High sensitivity high-resolution full range relaxometry using a fast mechanical sample shuttling device and a cryo-probe View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2016-10-15

AUTHORS

Ching-Yu Chou, Minglee Chu, Chi-Fon Chang, Tsunai Yu, Tai-huang Huang, Dimitris Sakellariou

ABSTRACT

Field-dependent NMR studies of bio-molecular systems using a sample shuttling hardware operating on a high-field NMR apparatus have provided valuable structural and dynamic information. We have recently published a design of a compact sample transportation device, called “field-cycler”, which was installed in a commercial spectrometer and which provided highly precise positioning and stability during high speed shuttling. In this communication, we demonstrate the first use of a sample shuttling device on a commercial high field standard bore NMR spectrometer, equipped with a commercial triple resonance cryogenically cooled NMR probe. The performance and robustness of the hardware operating in 1D and 2D field cycling experiments, as well as the impact of the sample shuttling time on the signal intensity are discussed. More... »

PAGES

187-194

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10858-016-0066-5

DOI

http://dx.doi.org/10.1007/s10858-016-0066-5

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1020874937

PUBMED

https://www.ncbi.nlm.nih.gov/pubmed/27744623


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