Cross-section transmission electron microscopy characterization of the near-surface structure of medical Nitinol superelastic tubing View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2007-03

AUTHORS

Pavel L. Potapov, Wim Tirry, Dominique Schryvers, Valerie G. M. Sivel, Meng-Yue Wu, Dimitri Aslanidis, Henny Zandbergen

ABSTRACT

The application of Nitinol in a wide variety of medical implants is progressively increasing because of its unique mechanical properties, durability and biocompatibility. However, as Nitinol consists of about 50 at.% of toxic Ni, certain applications are still hindered by the concern of free Ni release in the surrounding tissue. The latter is controlled by the structure of near-surface layers and can be strongly affected by various surface treatments. A proper application of advanced cross-section sample preparation techniques allows us to characterize the Nitinol near-surface structure down to the nanoscale by means of transmission electron microscopy (TEM). Elemental maps of the Ti, O and Ni distribution, concentration profiles, quantification of composition as well as atomic resolution images at the surface of a Nitinol tubing are presented and the results obtained with different sample preparation and analytical characterization techniques are compared. In addition to a strong decrease of Ni towards the surface of the oxide layer and a Ti depleted layer underneath the oxide, also a possible transformation from TiO to TiO(2) is documented. More... »

PAGES

483-492

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10856-007-2008-y

DOI

http://dx.doi.org/10.1007/s10856-007-2008-y

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1030578307

PUBMED

https://www.ncbi.nlm.nih.gov/pubmed/17334699


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