Preparation, structural and micromechanical properties of (Al/Mg) co-doped ZnO nanoparticles by sol–gel process View Full Text


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Article Info

DATE

2015-10

AUTHORS

E. Asikuzun, O. Ozturk, L. Arda, D. Akcan, S. D. Senol, C. Terzioglu

ABSTRACT

Zn0.90Mg0.10−xAlxO (x = 0.0, 0.1, 0.2, 0.3, 0.4, 0.5 and 0.10) nanoparticles were prepared by using sol–gel technique. The effects of Al and Mg doping on the structural and mechanical properties were investigated by using X-Ray diffraction (XRD), scanning electron microscopy (SEM) and digital micro-hardness tester, respectively. The grain size, a and c lattice parameters and morphology of nanoparticles were characterized by XRD and SEM measurements. The grain sizes of Al/Mg co-doped ZnO nanoparticles were also calculated by Scherrer–Warren equation. a and c lattice parameters are calculated from XRD peaks. According to the results it was observed that the grain sizes increased with increasing the Al doping. c lattice parameter partially decreased with Al doping. The experimental results of hardness measurements were analyzed using Meyer’s law, proportional specimen resistance model, elastic/plastic deformation model, and Hays–Kendall (HK) approach. It was observed that HK approach is the most successful model for the micro-hardness analysis of Al/Mg co-doped ZnO materials. More... »

PAGES

8147-8159

References to SciGraph publications

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    http://scigraph.springernature.com/pub.10.1007/s10854-015-3475-4

    DOI

    http://dx.doi.org/10.1007/s10854-015-3475-4

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