Microcrystalline Gd2MoO6 prepared by combined mechanochemical/thermal process and its magnetic properties View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2019-04

AUTHORS

Erika Tóthová, Róbert Tarasenko, Vladimír Tkáč, Martin Orendáč, Michal Hegedüs, Zuzana Danková, Marián Holub, Matej Baláž, Marek Matik

ABSTRACT

Gadolinium oxymolybdate, Gd2MoO6 (monoclinic, C2/c) was prepared via nonconventional mechanochemical/thermal process from powdered oxide precursors (Gd2O3 and (NH4)2MoO4). The effect of mechanical activation via high-energy ball milling on the reactivity of the stoichiometric Gd2O3 + (NH4)2MoO4 mixture was studied by thermal analysis (TG-DSC) and Fourier-transform infrared spectroscopy. While thermal treatment of nonactivated mixture leads only to decomposition of (NH4)2MoO4 and formation of Gd2O3–MoO3 system, mechanical activation provides enough energy for a chemical reaction between both reactants. The product with an average crystallite size of approximately 1 μm shows a well-faceted morphology. The investigation of magnetic properties revealed antiferromagnetic coupling, which is attributed to exchange interactions. More... »

PAGES

1-11

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http://scigraph.springernature.com/pub.10.1007/s10853-019-03331-z

DOI

http://dx.doi.org/10.1007/s10853-019-03331-z

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https://app.dimensions.ai/details/publication/pub.1111318062


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