Rapid mechanochemical synthesis of titanium and hafnium carbides View Full Text


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Article Info

DATE

2018-05-24

AUTHORS

Nikolay Lyakhov, Tatiana Grigoreva, Vladimir Šepelák, Boris Tolochko, Aleksey Ancharov, Sergey Vosmerikov, Evgeniya Devyatkina, Tatyana Udalova, Sofia Petrova

ABSTRACT

The mechanically triggered interactions in the Ti–C and Hf–C systems performed in a high-energy planetary ball mill are studied. The formation of carbides (TiC and HfC) in the course of mechanochemical synthesis at the different stages is followed by both conventional and synchrotron X-ray diffraction analyses and high-resolution scanning and transmission electron microscopy. The mechanism of the mechanochemically induced reactions in the Ti–C and Hf–C systems leading to the relatively rapid formation of TiC and HfC, respectively, is proposed. The interaction between metallic Ti (Hf) and C proceeds through the formation of mechanocomposites Ti/C (Hf/C) at the first stage, followed by the melting of titanium (hafnium), the spreading it over the carbon particle surface and the crystallization of titanium (hafnium) carbides. It is demonstrated that the mechanosynthesis of ultra-fine TiC and HfC is completed after 20 and 8 min of mechanical activation, respectively. More... »

PAGES

13584-13591

References to SciGraph publications

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URI

http://scigraph.springernature.com/pub.10.1007/s10853-018-2450-x

DOI

http://dx.doi.org/10.1007/s10853-018-2450-x

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172 grid-institutes:grid.415877.8 schema:alternateName G.I. Budker Institute of Nuclear Physics, Siberian Branch of Russian Academy of Sciences, Academician Lavrentiev Avenue 11, 630090, Novosibirsk, Russia
173 Institute of Solid State Chemistry and Mechanochemistry, Siberian Branch of Russian Academy of Sciences, Kutateladze Str. 18, 630128, Novosibirsk, Russia
174 schema:name G.I. Budker Institute of Nuclear Physics, Siberian Branch of Russian Academy of Sciences, Academician Lavrentiev Avenue 11, 630090, Novosibirsk, Russia
175 Institute of Solid State Chemistry and Mechanochemistry, Siberian Branch of Russian Academy of Sciences, Kutateladze Str. 18, 630128, Novosibirsk, Russia
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177 grid-institutes:grid.4605.7 schema:alternateName Novosibirsk State University, Pirogov Str. 2, 630090, Novosibirsk, Russia
178 schema:name G.I. Budker Institute of Nuclear Physics, Siberian Branch of Russian Academy of Sciences, Academician Lavrentiev Avenue 11, 630090, Novosibirsk, Russia
179 Institute of Solid State Chemistry and Mechanochemistry, Siberian Branch of Russian Academy of Sciences, Kutateladze Str. 18, 630128, Novosibirsk, Russia
180 Novosibirsk State University, Pirogov Str. 2, 630090, Novosibirsk, Russia
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182 grid-institutes:grid.465367.5 schema:alternateName Institute of Metallurgy, Ural Branch of Russian Academy of Sciences, Amundsen Str. 101, 620016, Ekaterinburg, Russia
183 schema:name Institute of Metallurgy, Ural Branch of Russian Academy of Sciences, Amundsen Str. 101, 620016, Ekaterinburg, Russia
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185 grid-institutes:grid.77667.37 schema:alternateName Novosibirsk State Technical University, K. Marx Avenue 20, 630073, Novosibirsk, Russia
186 schema:name Institute of Solid State Chemistry and Mechanochemistry, Siberian Branch of Russian Academy of Sciences, Kutateladze Str. 18, 630128, Novosibirsk, Russia
187 Novosibirsk State Technical University, K. Marx Avenue 20, 630073, Novosibirsk, Russia
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