Solid-state processing of oxidation-resistant molybdenum borosilicide composites for ultra-high-temperature applications View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2014-11

AUTHORS

Bruce A. Cook, Christopher A. Bonino, James A. Trainham

ABSTRACT

The high-temperature capabilities of multi-phase composites based on Mo5Si3Bx are examined after solid-state processing and pulsed laser deposition (PLD) coating fabrication approaches. These composites are prepared by mechanical alloying of elemental powders and densified by vacuum hot pressing, which is a scalable processing approach. Chemical analyses of the hot-pressed compacts reveal a consistent 15–22 percent loss of boron, which is primarily due to the high-temperature hot-pressing step. Composites possessing sufficient amounts of boron are evaluated by thermogravimetric studies in temperatures up to 1650 °C in air. One composition demonstrates oxidative stability after long-term (100 h) isothermal conditions, as well as thermal cycling to simulate solar-thermal operation. Hot-pressed samples of composites consisting of Mo5Si3Bx + MoSi2 + MoB are also employed as deposition targets for PLD trials. X-ray diffraction analysis of the resulting films indicates the absence of long-range crystallographic order. More... »

PAGES

7750-7759

Journal

TITLE

Journal of Materials Science

ISSUE

22

VOLUME

49

Author Affiliations

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10853-014-8485-8

DOI

http://dx.doi.org/10.1007/s10853-014-8485-8

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1006352828


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