Dispersion of gold dodecanethiolate in a silsesquioxane film with pendant dodecyl chains: from photoluminescent materials to gold nanocomposites View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2013-12

AUTHORS

María Lorena Gómez, Ignacio E. dell′Erba, Carlos A. Chesta, Cristina E. Hoppe, Roberto J. J. Williams

ABSTRACT

Photoluminescence of Au(I)-dodecane thiolate (Au(I)-DDT) and its thermal reduction to metallic gold have been extensively reported in the literature. However, the incorporation of this salt to a polymeric matrix to produce photoluminescent materials or gold nanocomposites by thermal reduction is a difficult task due to the insolubility of Au(I)-DDT. In this study it is shown that a silsesquioxane with pendant dodecyl chains can be a convenient host of Au(I)-DDT. The presence of dodecyl chains in both compounds and the in situ generation of the salt in the solution of the silsesquioxane precursor enabled to obtain a uniform dispersion of Au(I)-DDT in the silsesquioxane matrix. Flexible films were generated, exhibiting characteristic photoluminescent properties before thermal treatment and a uniform dispersion of gold nanoparticles after heating at 150 °C for different periods of time. More... »

PAGES

8559-8565

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10853-013-7675-0

DOI

http://dx.doi.org/10.1007/s10853-013-7675-0

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1019900215


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