Copper crystals on the (110) sapphire plane: orientation relationships, triple line ridges and interface shape equilibrium View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2013-04

AUTHORS

Stefano Curiotto, Harry Chien, Hila Meltzman, Stephane Labat, Paul Wynblatt, Gregory S. Rohrer, Wayne D. Kaplan, Dominique Chatain

ABSTRACT

The orientation relationships (ORs) of copper crystals on a sapphire substrate equilibrated at 1253 K are presented. They barely depend on the procedures used in sample preparation, i.e. dewetting of a copper film in the liquid state or in the solid state. The most frequent OR found is Cu(111) || Al2O3 and Cu within few degrees from Al2O3[0001]. A secondary, lower frequency OR is also observed: Cu(001) || Al2O3 with Cu within a few degrees from either Al2O3 or Al2O3[0001]. These ORs do not follow the Fecht and Gleiter model which proposes that dense directions of the metal should align with dense directions of the oxide. On annealing, even at a temperature about half of the melting point of sapphire, fast diffusion of sapphire at the copper/sapphire interface is observed: the copper particles tend to achieve their interfacial equilibrium shapes by sinking into the substrate, and sapphire ridges form at the triple line. Finally, it is shown that the Cu(111) || Al2O3 interface remains flat at the atomic scale, and is therefore part of the copper/sapphire equilibrium interfacial shape. More... »

PAGES

3013-3026

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10853-012-7080-0

DOI

http://dx.doi.org/10.1007/s10853-012-7080-0

DIMENSIONS

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