Shape controllable preparation and characterization of hierarchical PbS submicron cubes via a solvothermal method View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2010-01

AUTHORS

Fei Li, Qinghua Qin, Jianfang Wu, Zhen Li

ABSTRACT

The controlled synthesis of PbS nanostructures with crystal morphology of hierarchical submicron cubes has been realized by chemical synthesis between lead acetate trihydrate and sulfur via a solvothermal route. X-ray diffraction, scanning electron microscopy, and transmission electron microscopy were used to characterize the products. It was shown that well-dispersed and hierarchical PbS submicron cubes were formed at low temperature. Experiments demonstrated that the morphologies of PbS crystals were significantly influenced by treatment temperature, reaction time, and sulfur sources. A growth model was proposed for the selective formation of hierarchical PbS submicron cubes. Our work demonstrated the growth of hierarchical PbS architectures through a one-step, surfactant-free and solution-phase chemical route under controlled conditions. More... »

PAGES

348-353

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10853-009-3942-5

DOI

http://dx.doi.org/10.1007/s10853-009-3942-5

DIMENSIONS

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