Confined palladium colloids in mesoporous frameworks for carbon nanotube growth View Full Text


Ontology type: schema:ScholarlyArticle      Open Access: True


Article Info

DATE

2009-12

AUTHORS

Angel Berenguer-Murcia, Evgeny V. Rebrov, Maciej Cabaj, Andrew E. H. Wheatley, Brian F. G. Johnson, John Robertson, Jaap C. Schouten

ABSTRACT

Palladium colloidal nanoparticles with an average size of approximately 2.4 nm have been incorporated into mesoporous inorganic thin films following a multistep approach. This involves the deposition of mesoporous titania thin films with a thickness of 200 nm by spin-coating on titanium plates with a superhydrophilic titania outer layer and activation by calcination in a vacuum furnace at 573 K. Nanoparticles have been confined within the porous titania network by dip-coating noble metal suspensions onto these mesoporous thin films. Finally, the resulting nanoconfined systems were used as substrates for the growth of oriented carbon nanotubes (CNTs) using plasma-enhanced chemical vapour deposition at 923 K in order to enhance their surface area. These CNTs were tested in the hydrogenation of phenylacetylene by hydrogen in a batch reactor. The initial reaction rate observed on a CNT/TiO2 structured catalyst was considerably higher than that on 1 wt% Pd/TiO2 thin films. More... »

PAGES

6563-6570

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10853-009-3629-y

DOI

http://dx.doi.org/10.1007/s10853-009-3629-y

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1008617745


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40 schema:description Palladium colloidal nanoparticles with an average size of approximately 2.4 nm have been incorporated into mesoporous inorganic thin films following a multistep approach. This involves the deposition of mesoporous titania thin films with a thickness of 200 nm by spin-coating on titanium plates with a superhydrophilic titania outer layer and activation by calcination in a vacuum furnace at 573 K. Nanoparticles have been confined within the porous titania network by dip-coating noble metal suspensions onto these mesoporous thin films. Finally, the resulting nanoconfined systems were used as substrates for the growth of oriented carbon nanotubes (CNTs) using plasma-enhanced chemical vapour deposition at 923 K in order to enhance their surface area. These CNTs were tested in the hydrogenation of phenylacetylene by hydrogen in a batch reactor. The initial reaction rate observed on a CNT/TiO2 structured catalyst was considerably higher than that on 1 wt% Pd/TiO2 thin films.
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