Preparation of nanocrystalline TiO2 porous films from terpineol-ethanol-PEG system View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2006-04

AUTHORS

Shaojing Bu, Zhengguo Jin, Xiaoxin Liu, Tao Yin, Zhijie Cheng

ABSTRACT

Nanocrystalline TiO2 porous films were prepared by a sol-gel dip coating method from a solution using poly(ethylene glycol) as a template, ethanol as a solvent and terpineol as a highly viscous solvent. The thickness of films increases greatly by increasing the amount of terpineol. However, the overmuch incorporation of terpineol hinders the formation of porous structure and accelerates the crack creation. The crack-free film having a three-dimensionally extended porous structure was obtained at the ethanol/terpineol ratio of 8:1, the film thickness with three depositions being 2.5 μm. Pretreatment of the precursor at an appropriate temperature also plays an important role in pore formation. Single-phase anatase TiO2 porous films were obtained after calcinations at 550°C for 1 h, and the crystal size increases with an increase in the amount of terpineol. The pore formation mechanism is discussed primarily in relation to the phase separation in the system and self-assembly of PEG. More... »

PAGES

2067-2073

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10853-006-8000-y

DOI

http://dx.doi.org/10.1007/s10853-006-8000-y

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1042079780


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