Liquid–liquid extraction studies with 4,4′-biphenylene-spaced bis-β-diketones View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2011-12

AUTHORS

Jack K. Clegg, Bianca Antonioli, David J. Bray, Karsten Gloe, Kerstin Gloe, Katrina A. Jolliffe, Olga N. Kataeva, George V. Meehan, Marco Wenzel

ABSTRACT

4,4′-biphenylene spaced lipophilic bis-β-diketone ligands of the type 4,4′-bis(RC(O)CH2C(O))C12H8 (R = Pr, Ph, hexyl, octyl, nonyl) have been prepared and used for the liquid–liquid extraction of d-block metal ions. These ligands are expected to interact with divalent metal ions to form charge-neutral trinuclear metallocycles of type [M3(L3)3(solvent)] as has been demonstrated with the previously reported derivative of H2L3 (R = tBu), the X-ray structure of which is reported. Liquid–liquid extraction studies were performed in a two-phase water/chloroform system employing a radiotracer technique for cobalt(II) and zinc(II). These experiments involved the systematic variation of ligand, metal and 4-ethylpyridine concentrations to probe the stoichiometries of the species extracted. Synergistic extraction was observed when 4-ethylpyridine was present with the ligand in the organic phase. Competitive extraction studies demonstrated the ligands are highly selective for copper(II) over cobalt(II), nickel(II), zinc(II) and cadmium(II). More... »

PAGES

319-329

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10847-011-9954-1

DOI

http://dx.doi.org/10.1007/s10847-011-9954-1

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1032670100


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