Complexation of metal ions with the novel diazadithia crown ether carrying two anthryl pendants in acetonitrile–tetrahydrofuran View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2009-10-15

AUTHORS

Semanur Parlayan, Aysel Başoğlu, Miraç Ocak, Hakan Alp, Halit Kantekin, Ümmühan Ocak

ABSTRACT

A new crown ether carrying two anthryl groups with nitrogen–sulfur donor atom was designed and synthesized by the reaction of the corresponding macrocyclic compound and 9-chloromethyl anthracene. The influence of metal cations such as Al3+, Zn2+, Fe2+, Fe3+, Co2+, Ni2+, Mn2+, Cu2+, Cd2+, Hg2+ and Pb2+ on the spectroscopic properties of the ligand was investigated in acetonitrile–tetrahydofuran solution (1/1) by means of absorption and emission spectrometry. Absorption spectra show isosbestic points in the spectrophotometric titration of Fe2+, Fe3+, Al3+, Cu2+ and Hg2+. The results of spectrophotometric titration experiments disclosed the complexation stoichiometry and complex stability constant of the novel ligand with Fe2+, Fe3+, Al3+, Cu2+and Hg2+cations. The presence of excess amounts of Al3+, Zn2+, Fe2+, Fe3+, Co2+, Ni2+, Mn2+, Cu2+, Cd2+, Hg2+ and Pb2+ cations caused an enhancement of anthryl fluorescence. The ligand showed good sensitivity for Zn2+ with respect to other metal cations with linear range and detection limit of 1.4 × 10−7 to 4.1 × 10−6 M and 1.0 × 10−8 M respectively. More... »

PAGES

133-140

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10847-009-9688-5

DOI

http://dx.doi.org/10.1007/s10847-009-9688-5

DIMENSIONS

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