A facial microwave-assisted synthesis, spectroscopic characterization and preliminary complexation studies of calix[4]pyrroles containing the hydroxamic-acid moiety View Full Text


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Article Info

DATE

2008-10

AUTHORS

Vinod K. Jain, Hiren C. Mandalia, Eringathodi Suresh

ABSTRACT

The synthesis, spectroscopic characterization and preliminary complexation properties of functionalized calix[4]pyrroles are described. To date, two generalized preparative approaches have been pursued (i) modifying the basic pyrrole-plus-ketone synthesis of calix[4]pyrrole by using microwave irradiation protocol, (ii) the basic meso-tetra(methyl) meso-tetra(p-nitrophenyl) calix[4]pyrrole skeleton was functionalized to give hydroxamic acids, especially in the meso-position of the macrocycles. The structures of novel calix[4]pyrrole hydroxamic acid derivatives were confirmed on the basis of various physico-chemical techniques such as elemental analysis, FT-IR, 1H NMR and FAB-Mass. The results of preliminary studies on the extraction of vanadium (V) with the host calix[4]pyrrole hydroxamic acids were elucidated by significant examination of UV–Vis spectroscopy and ICP-AES. Single crystal structure of basic meso-tetra(methyl) meso-tetra (p-nitro phenyl) calix[4]pyrrole moiety has also been reported. More... »

PAGES

167

References to SciGraph publications

  • 2004-06. Heterocalixarenes. (Review) in CHEMISTRY OF HETEROCYCLIC COMPOUNDS
  • 2001-06. Synthesis and Extraction Properties of 1,3,5-O-trimethyl-2,4,6-tri-O-hydroxamic Acid p-tert-butyl Calix[6]arene in JOURNAL OF INCLUSION PHENOMENA AND MACROCYCLIC CHEMISTRY
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    http://scigraph.springernature.com/pub.10.1007/s10847-008-9453-1

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    http://dx.doi.org/10.1007/s10847-008-9453-1

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