Structure of Dibenzocrown Ethers and their H-Bonded Adducts.1. [1.5]Dibenzo-18-Crown-6 and Biphenyl-20-Crown-6: Complexes with Amidosulfuric Acid View Full Text


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Article Info

DATE

2005-06

AUTHORS

Sergei A. Kotlyar, Marina S. Fonari, Yurii A. Simonov, Gabriele Bocelli, Oleg V. Shishkin, Svetlana V. Shishkina, Vyacheslav V. Tkachuk, Ruslan Ya. Grygorash, Gerbert L. Kamalov

ABSTRACT

The interaction of the amidosulfuric acid NH3SO3 with 15 distal and proximal dibenzocrown ethers, including diphenyloxide, diphenylsulfide and biphenyl ones leads to the stable (1:1) complexes only in the case of [2.4]- and [1.5]dibenzo-18-crown-6 and biphenyl-20-crown-6. According to the data of the X-ray analysis, in the two last adducts the amidosulfuric acid coordinates to hexadentate crown ethers in a zwitterion form through a near-ideal ‘tripod’ arrangement to alternate crown oxygen atoms. The conformations of crown molecules are different in complexes and in initial macrocyclic ligands. More... »

PAGES

75-84

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10847-004-5208-9

DOI

http://dx.doi.org/10.1007/s10847-004-5208-9

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1039693303


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