A novel hybrid nanoparticle based on Fe3O4/TMAOH/poly(L-co-D,L lactic acid-co-trimethylene carbonate) prepared through the solvent displacement method View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2019-06

AUTHORS

Vagner de Oliveira Machado, Ângela Leão Andrade, Luis Carlos Duarte Cavalcante, José Domingos Fabris, Rosana Zacarias Domingues, José Domingos Ardisson, Luís E. Fernandez-Outon, Carmen Pizarro, Carlos Nelson Elias

ABSTRACT

TMAOH-dispersed nanoparticles of magnetite were first prepared through the reduction–precipitation of ferric chloride with Na2SO3 and NH4OH. The TMAOH-dispersed (Fe3O4) magnetic nanoparticles were then surface-coated with poly(L-co-D,L lactic acid-co-trimethylene carbonate) (PLDLA-co-TMC) to obtain the corresponding hybrid system (Fe3O4/TMAOH/PLDLA-co-TMC). Samples of so prepared material were analyzed by Fourier-transform infrared spectroscopy (FTIR), powder X-ray diffraction (XRD), magnetization measurements up to 2.5 T, and Mössbauer spectroscopy. Results indicate that this magnetic iron oxide soon after the synthesis is structurally close enough to a typically pure stoichiometric magnetite. FTIR data support clears evidences confirming the efficiency of the solvent displacement method to assure coating the TMAOH-dispersed (Fe3O4) magnetic nanoparticles with the terpolymer while preserves the main chemical structural characteristic of the nanosized magnetite. More... »

PAGES

21

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10751-019-1558-y

DOI

http://dx.doi.org/10.1007/s10751-019-1558-y

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https://app.dimensions.ai/details/publication/pub.1112685195


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