Lattice dynamics of Li2FeSiO4/C from 57Fe Mössbauer spectroscopy View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2019-06

AUTHORS

Juan Antonio Jaén, María Pino

ABSTRACT

Lithium Iron (II) Silicate, Li2FeSiO4, is a promising cathode material for Li-ion battery applications. Its carbon composite Li2FeSiO4/C was synthesized by a simple dry ball-milling process combined with high- temperature treatment, using citric acid as carbon source, and characterized by temperature-dependence. Powder X-ray diffraction shows that it crystallizes in a monoclinic structure with (P21/n) symmetry. 57Fe Mössbauer effect studies in the temperature range 16.5–298 K were carried out. The temperature dependence of the isomer shifts was used to estimate the effective vibrating mass, Meff, yielding a value of ~87 g mol−1 for Fe in the FeO42-- moiety. This is due to the significant covalency of the Fe-0 bond in the orthosilicate composite. The temperature dependence of the recoil-free fraction (spectral areas), when combined with the effective vibrating mass calculation, yields the “Mössbauer lattice temperature” of θM = 165 K Low temperatures reveals that paramagnetic Li2FeSiO4/C becomes antiferromagnetic at 16.5 K. More... »

PAGES

16

Journal

TITLE

Hyperfine Interactions

ISSUE

1

VOLUME

240

Author Affiliations

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10751-019-1555-1

DOI

http://dx.doi.org/10.1007/s10751-019-1555-1

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https://app.dimensions.ai/details/publication/pub.1112261981


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