Mossbauer spectroscopy study of Fe@ZrO2 nanocomposites formation by MA SHS technology View Full Text


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Article Info

DATE

2018-12

AUTHORS

Tatiana Kiseleva, Alexey Letsko, Tatiana Talako, Svetlana Kovaleva, Tatiana Grigoreva, Alla Novakova, Nikolay Lyakhov

ABSTRACT

Particles with core-in-shell structure Fe@ZrO2 were synthesized by step-by-step technology including formation of mechanically pre-activated (MA) precursors with Fe/Zr and Fe2O3/[Fe/Zr] composite structures formation following by Self-Propagated High temperature synthesis (SHS). Mossbauer spectroscopy, Transmission and Scanning electron Microscopy have been performed to study the peculiarities of local structure and its evolution through the sequential synthesis steps via various milling periods and reagent compositions. The exact conditions for iron core in oxide shell Fe@ZrO2 structure formation with promising functionality has been established. More... »

PAGES

14

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10751-018-1490-6

DOI

http://dx.doi.org/10.1007/s10751-018-1490-6

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1100820700


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