Evolution under thermal annealing of Mn-doped iron disilicides obtained by ball milling View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2007-07

AUTHORS

J. Martínez, J. Runco, S. M. Cotes, M. A. Taylor, J. Desimoni

ABSTRACT

Phase formation in the Mn doped -FeSi2 system (Fe1 − xMnxSi2, with 0.00 ≤ x ≤ 0.24) was studied using X-ray diffraction and Mössbauer spectroscopy. Samples were prepared by the simultaneous mill of pure Si, Mn and Fe under Ar atmosphere followed by an annealing at 1,123 K during 4 h at 1 × 10 − 7 Torr. After milling, an admixture of -FeSi2, -FeSi2 and -FeSi phases was present while -FeSi2 disappeared after annealing, resulting -FeSi2 the main phase. Depending on Mn concentration, small amounts of -FeSi and Si segregation were also observed. A preferential substitution of Fe atoms by Mn ones in the FeII site of the -FeSi2 regular lattice was inferred from the Mössbauer results. More... »

PAGES

13-17

References to SciGraph publications

Journal

TITLE

Hyperfine Interactions

ISSUE

1-3

VOLUME

178

Author Affiliations

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10751-008-9649-1

DOI

http://dx.doi.org/10.1007/s10751-008-9649-1

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1014050936


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